Tricyclo[6.3.1.02,5]dodecan-9-ol,1-[(2'-hydroxy-5,5'-di-2-propen-1-yl[1,1'-biphenyl]-2-yl)oxy]-4,4,8-trimethyl-,(1R,2S,5R,8S,9S)-

Base Information

Chemical Name:Tricyclo[6.3.1.02,5]dodecan-9-ol,1-[(2'-hydroxy-5,5'-di-2-propen-1-yl[1,1'-biphenyl]-2-yl)oxy]-4,4,8-trimethyl-,(1R,2S,5R,8S,9S)-
CAS No.:133056-11-8
Molecular Formula:C33H42 O3
Molecular Weight:486.695
Hs Code.:

Synonyms:Tricyclo[6.3.1.02,5]dodecan-9-ol,1-[(2'-hydroxy-5,5'-di-2-propenyl[1,1'-biphenyl]-2-yl)oxy]-4,4,8-trimethyl-,(1R,2S,5R,8S,9S)- (9CI); Tricyclo[6.3.1.02,5]dodecan-9-ol,1-[(2'-hydroxy-5,5'-di-2-propenyl[1,1'-biphenyl]-2-yl)oxy]-4,4,8-trimethyl-,[1R-(1a,2a,5b,8b,9b)]-; (+)-Caryolanemagnolol; Caryolanemagnolol

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Chemical Property of Tricyclo[6.3.1.02,5]dodecan-9-ol,1-[(2'-hydroxy-5,5'-di-2-propen-1-yl[1,1'-biphenyl]-2-yl)oxy]-4,4,8-trimethyl-,(1R,2S,5R,8S,9S)-

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MSDS Files:: SDS file from LookChem

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Technology Process of Tricyclo[6.3.1.02,5]dodecan-9-ol,1-[(2'-hydroxy-5,5'-di-2-propen-1-yl[1,1'-biphenyl]-2-yl)oxy]-4,4,8-trimethyl-,(1R,2S,5R,8S,9S)-

There total 13 articles about Tricyclo[6.3.1.02,5]dodecan-9-ol,1-[(2'-hydroxy-5,5'-di-2-propen-1-yl[1,1'-biphenyl]-2-yl)oxy]-4,4,8-trimethyl-,(1R,2S,5R,8S,9S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1213270-07-5
C₄₀H₅₃NO₅

: 133056-11-8
caryolanemagnolol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 23 - 65 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol100214X

Reference yield: 15.0%

: 528-43-8
Magnolol

: 87-44-5
β-caryophyllene

: 130756-35-3
clovanemagnolol

: 133056-11-8
caryolanemagnolol

Guidance literature:: β-caryophyllene; With oxone; (3aS,4'R,7aS)-2,2,2',2'-tetramethyldihydrospiro[[1,3]dioxolo-[4,5-c]pyran-6,4'-[1,3]dioxolan]-7(7aH)-one; In Dimethoxymethane; acetonitrile; at 0 ℃; pH=10.5; aq. buffer; Inert atmosphere;

Magnolol; With diphenyl hydrogen phosphate; In dichloromethane; at 23 - 38 ℃; for 2.55h; Inert atmosphere;
DOI:10.1021/ol100214X