Technology Process of C30H32N2O2
There total 8 articles about C30H32N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(9-(3-(benzyl(tert-butoxycarbonyl)amino)propyl)-2,3,4,9-tetrahydro-1H-carbazol-6-yl)methyl benzoate;
With
hydrogenchloride;
In
ethyl acetate;
at 20 ℃;
for 2h;
With
sodium carbonate;
In
ethyl acetate;
DOI:10.1039/c2md20211e
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: N-Bromosuccinimide; ammonium acetate / diethyl ether / 0.5 h / 20 °C
2.1: 2-methoxy-ethanol / 12 h / 130 °C / Inert atmosphere
3.1: potassium hydroxide / dimethyl sulfoxide / 3 h / 20 °C
4.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C
5.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C
5.2: 1 h
6.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C
7.1: triethylamine / dichloromethane / 12 h / 20 °C
8.1: hydrogenchloride / ethyl acetate / 2 h / 20 °C
With
hydrogenchloride; N-Bromosuccinimide; lithium aluminium tetrahydride; ammonium acetate; potassium carbonate; triethylamine; potassium hydroxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; 2-methoxy-ethanol; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c2md20211e
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium hydroxide / dimethyl sulfoxide / 3 h / 20 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C
3.2: 1 h
4.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C
5.1: triethylamine / dichloromethane / 12 h / 20 °C
6.1: hydrogenchloride / ethyl acetate / 2 h / 20 °C
With
hydrogenchloride; lithium aluminium tetrahydride; potassium carbonate; triethylamine; potassium hydroxide;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c2md20211e
