C₆₈H₁₀₆O₁₅Si₂

Base Information

Chemical Name:C₆₈H₁₀₆O₁₅Si₂
CAS No.:247146-68-5
Molecular Formula:C₆₈H₁₀₆O₁₅Si₂
Molecular Weight:1219.75
Hs Code.:

C<sub>68</sub>H<sub>106</sub>O<sub>15</sub>Si<sub>2</sub>

Synonyms:C₆₈H₁₀₆O₁₅Si₂

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Chemical Property of C₆₈H₁₀₆O₁₅Si₂

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Technology Process of C₆₈H₁₀₆O₁₅Si₂

There total 3 articles about C₆₈H₁₀₆O₁₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 994-30-9
triethylsilyl chloride

: 215876-26-9
C₅₆H₇₈O₁₅

: C₆₂H₉₂O₁₅Si

: C₆₂H₉₂O₁₅Si

: 247146-68-5
C₆₈H₁₀₆O₁₅Si₂

: C₇₄H₁₂₀O₁₅Si₃

Guidance literature:: With dmap; In dichloromethane; at -10 ℃; Further byproducts given. Yields of byproduct given;
DOI:10.1002/(SICI)1521-3773(19980918)37:17<2354::AID-ANIE2354>3.0.CO;2-9

Reference yield:

: 215876-25-8
C₇₉H₁₃₂O₁₅Si₄

: 247146-68-5
C₆₈H₁₀₆O₁₅Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: HF*pyr; pyridine / tetrahydrofuran / 72 h

2: 65 percent / DMAP / CH₂Cl₂ / 10 °C

With pyridine; dmap; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane; 1: Cyclization / 2: silylation;
DOI:10.1021/ja990860j

Reference yield:

: 994-30-9
triethylsilyl chloride

: 215876-26-9
C₅₆H₇₈O₁₅

: C₆₂H₉₂O₁₅Si

: C₆₂H₉₂O₁₅Si

: C₆₂H₉₂O₁₅Si

: 247146-68-5
C₆₈H₁₀₆O₁₅Si₂

Guidance literature:: With dmap; In dichloromethane; at -10 ℃; Yield given; Further byproducts given. Yields of byproduct given;
DOI:10.1002/(SICI)1521-3773(19980918)37:17<2354::AID-ANIE2354>3.0.CO;2-9