triphenylphosphine monomethylborane adduct

Base Information

• Chemical Name: triphenylphosphine monomethylborane adduct
• CAS No.: 79840-24-7
• Molecular Formula: CH₅B*C₁₈H₁₅P
• Molecular Weight: 290.153

Synonyms:triphenylphosphine monomethylborane adduct

Chemical Property of triphenylphosphine monomethylborane adduct

Chemical Property:

Purity/Quality:

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Technology Process of triphenylphosphine monomethylborane adduct

There total 3 articles about triphenylphosphine monomethylborane adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methylenetriphenylphosphorane-borane (16510-42-2) → triphenylphosphine monomethylborane adduct (79840-24-7)

Guidance literature:

In chlorobenzene; moisture and air-oxygen exclusion, heating (131°C, 420 min); solvent removal (room temp., high vacuum);

Reference yield: 95.0%

methylenetriphenylphosphorane-borane (16510-42-2) → CH3BH2P(C6H5)3=CH3BH2*P(C6H5)3 (79840-24-7) + methylborane (12538-96-4)

Guidance literature:

In chlorobenzene; byproducts: PPh3; heated at 131°C for 7 h;

Reference yield:

methylborane (12538-96-4) → CH3BH2P(C6H5)3=CH3BH2*P(C6H5)3 (79840-24-7)

Guidance literature:

With triphenylphosphine; at 25°C;

upstream raw materials:

methylenetriphenylphosphorane-borane

methylborane

Downstream raw materials:

1,1-dicyclohexylethanol

trimethylborane

triphenylphosphine

B-Methyl-dicyclohexyl-boran

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