<(S)-1-Benzyl-2-<(S)-2-(3,3-dimethyl-2-oxobutyl)-pyrrolodino>-2-oxoethyl>-2,2-dimethylpropionat

Base Information

Chemical Name:<(S)-1-Benzyl-2-<(S)-2-(3,3-dimethyl-2-oxobutyl)-pyrrolodino>-2-oxoethyl>-2,2-dimethylpropionat
CAS No.:121378-47-0
Molecular Formula:C₂₄H₃₅NO₄
Molecular Weight:401.546
Hs Code.:

Synonyms:<(S)-1-Benzyl-2-<(S)-2-(3,3-dimethyl-2-oxobutyl)-pyrrolodino>-2-oxoethyl>-2,2-dimethylpropionat

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Chemical Property of <(S)-1-Benzyl-2-<(S)-2-(3,3-dimethyl-2-oxobutyl)-pyrrolodino>-2-oxoethyl>-2,2-dimethylpropionat

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Technology Process of <(S)-1-Benzyl-2-<(S)-2-(3,3-dimethyl-2-oxobutyl)-pyrrolodino>-2-oxoethyl>-2,2-dimethylpropionat

There total 3 articles about <(S)-1-Benzyl-2-<(S)-2-(3,3-dimethyl-2-oxobutyl)-pyrrolodino>-2-oxoethyl>-2,2-dimethylpropionat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 17510-46-2
3,3-dimethyl-2-(trimethylsilyl)oxy-1-butene

: 121378-62-9,121395-80-0,132255-67-5
<(S)-1-Benzyl-2-<2-methoxypyrrolidino>-2-oxoethyl>-2,2-dimethylpropionat

: 121378-48-1
<(S)-1-Benzyl-2-<(R)-2-(3,3-dimethyl-2-oxobutyl)-pyrrolodino>-2-oxoethyl>-2,2-dimethylpropionat

: 121378-47-0
<(S)-1-Benzyl-2-<(S)-2-(3,3-dimethyl-2-oxobutyl)-pyrrolodino>-2-oxoethyl>-2,2-dimethylpropionat

Guidance literature:: titanium tetrachloride; In dichloromethane; Yields of byproduct given;
DOI:10.1002/ardp.19893220209

Reference yield:

: 17510-46-2
3,3-dimethyl-2-(trimethylsilyl)oxy-1-butene

: 121378-47-0
<(S)-1-Benzyl-2-<(S)-2-(3,3-dimethyl-2-oxobutyl)-pyrrolodino>-2-oxoethyl>-2,2-dimethylpropionat

Guidance literature:: Multi-step reaction with 2 steps

1: 7.4 percent / TiCl₄ / acetonitrile / 18 h / 0 °C

2: 55 percent / NEt₃ / tetrahydrofuran

With titanium tetrachloride; triethylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1002/ardp.19893220209

Reference yield:

: (S)-2-Benzyl-5,6,7,7a-tetrahydro-pyrrolo<2,1-b>oxazol-3(2H)-on

: 121378-47-0
<(S)-1-Benzyl-2-<(S)-2-(3,3-dimethyl-2-oxobutyl)-pyrrolodino>-2-oxoethyl>-2,2-dimethylpropionat

Guidance literature:: Multi-step reaction with 2 steps

1: 7.4 percent / TiCl₄ / acetonitrile / 18 h / 0 °C

2: 55 percent / NEt₃ / tetrahydrofuran

With titanium tetrachloride; triethylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1002/ardp.19893220209