sodium N-(P,P-diphenylphosphinoyl)-P,P-diphenylphosphinimidate

Base Information

• Chemical Name: sodium N-(P,P-diphenylphosphinoyl)-P,P-diphenylphosphinimidate
• CAS No.: 135823-11-9
• Molecular Formula: C₂₄H₂₀NO₂P₂*Na
• Molecular Weight: 439.366
• Mol file: 135823-11-9.mol

Synonyms:sodium N-(P,P-diphenylphosphinoyl)-P,P-diphenylphosphinimidate

Chemical Property of sodium N-(P,P-diphenylphosphinoyl)-P,P-diphenylphosphinimidate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of sodium N-(P,P-diphenylphosphinoyl)-P,P-diphenylphosphinimidate

There total 1 articles about sodium N-(P,P-diphenylphosphinoyl)-P,P-diphenylphosphinimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

imidotetraphenyldiphosphinic acid (31239-06-2) → sodium N-(P,P-diphenylphosphinoyl)-P,P-diphenylphosphinimidate (135823-11-9)

Guidance literature:

With sodium ethanolate; In ethanol;

Reference yield: 100.0%

dichlorophenylstibine (5035-52-9) + sodium N-(P,P-diphenylphosphinoyl)-P,P-diphenylphosphinimidate (135823-11-9) → PhSbCl((OPPh2)2N)

Guidance literature:

In chloroform; byproducts: NaCl; react. PhSbCl2 and Na((OPPh2)2N) (1:1) in CHCl3 for 6 h under Ar; soln. was filtered and evapd.; elem. anal.;

DOI:10.1016/S0022-328X(01)01198-6

Reference yield: 95.0%

rhenium(I) pentacarbonyl bromide (14220-21-4) + sodium N-(P,P-diphenylphosphinoyl)-P,P-diphenylphosphinimidate (135823-11-9) → Na[Re2(CO)6(μ-Ph2P(O)NP(O)Ph2-κ2O)2]

Guidance literature:

In toluene; byproducts: CO, NaBr; treatment of equimolar amts. of ReBr(CO)5 with Na(Ph2P(O)NP(O)Ph2) in boiling toluene;

DOI:10.1021/om050912f

upstream raw materials:

imidotetraphenyldiphosphinic acid

Downstream raw materials:

(tetraphenylimidodiphosphinato)trimethyllead(IV)

(CO)4Mn(N(P(O)(C₆H₅)2)2)