methyl N²-[(benzyloxy)carbonyl]-N⁶-{[4,7,10-tris-(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecan-1-yl]acetyl}-L-lysinate

Base Information

• Chemical Name: methyl N²-[(benzyloxy)carbonyl]-N⁶-{[4,7,10-tris-(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecan-1-yl]acetyl}-L-lysinate
• CAS No.: 640731-06-2
• Molecular Formula: C₄₀H₆₆N₆O₁₁
• Molecular Weight: 806.998

Synonyms:methyl N²-[(benzyloxy)carbonyl]-N⁶-{[4,7,10-tris-(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecan-1-yl]acetyl}-L-lysinate

Chemical Property of methyl N²-[(benzyloxy)carbonyl]-N⁶-{[4,7,10-tris-(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecan-1-yl]acetyl}-L-lysinate

Chemical Property:

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Technology Process of methyl N²-[(benzyloxy)carbonyl]-N⁶-{[4,7,10-tris-(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecan-1-yl]acetyl}-L-lysinate

There total 1 articles about methyl N²-[(benzyloxy)carbonyl]-N⁶-{[4,7,10-tris-(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecan-1-yl]acetyl}-L-lysinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-methyl 6-amino-2-(benzyloxycarbonylamino)hexanoate (5591-93-5) + 2-(4,7,10-tris(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecan-1-yl)acetic acid (247193-74-4) → methyl N2-[(benzyloxy)carbonyl]-N6-{[4,7,10-tris-(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecan-1-yl]acetyl}-L-lysinate (640731-06-2)

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 6h;

DOI:10.1021/ja034730t

upstream raw materials:

(S)-methyl 6-amino-2-(benzyloxycarbonylamino)hexanoate

2-(4,7,10-tris(tert-butoxycarbonyl)-1,4,7,10-tetraazacyclododecan-1-yl)acetic acid

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