methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-azidoethoxy)ethoxy]phenyl}-α-D-glucopyranoside

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Chemical Name:methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-azidoethoxy)ethoxy]phenyl}-α-D-glucopyranoside
CAS No.:1352299-26-3
Molecular Formula:C₃₈H₄₃N₃O₈
Molecular Weight:669.775
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-azidoethoxy)ethoxy]phenyl}-α-D-glucopyranoside

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Chemical Property of methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-azidoethoxy)ethoxy]phenyl}-α-D-glucopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-azidoethoxy)ethoxy]phenyl}-α-D-glucopyranoside

There total 3 articles about methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-azidoethoxy)ethoxy]phenyl}-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1352299-25-2
4-[2-(2-azidoethoxy)ethoxy]phenol

: 114219-26-0
methyl 2,3,4-tri-O-benzyl-6-O-(4-methylbenzenesulfonyl)-α-D-glucopyranoside

: 1352299-26-3
methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-azidoethoxy)ethoxy]phenyl}-α-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 70 ℃; for 3h;
DOI:10.1016/j.tet.2011.09.030

Reference yield:

: C₁₅H₂₁N₃O₄

: 1352299-26-3
methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-azidoethoxy)ethoxy]phenyl}-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: camphor-10-sulfonic acid / tetrahydrofuran; methanol / 0.08 h / 20 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 3 h / 70 °C

With camphor-10-sulfonic acid; sodium hydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.09.030

Reference yield:

: 53936-56-4
4-(tetrahydro-2H-2-pyranyloxy)phenol

: 1352299-26-3
methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-azidoethoxy)ethoxy]phenyl}-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 30 h / 70 °C / Inert atmosphere

1.2: 30 h / 70 °C / Inert atmosphere

2.1: camphor-10-sulfonic acid / tetrahydrofuran; methanol / 0.08 h / 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide / 3 h / 70 °C

With camphor-10-sulfonic acid; sodium hydride; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.09.030