1-(4-bromobenzyloxy)octane

Base Information

Chemical Name:1-(4-bromobenzyloxy)octane
CAS No.:1410119-96-8
Molecular Formula:C₁₅H₂₃BrO
Molecular Weight:299.251
Hs Code.:

Synonyms:1-(4-bromobenzyloxy)octane

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Chemical Property of 1-(4-bromobenzyloxy)octane

Chemical Property:

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Technology Process of 1-(4-bromobenzyloxy)octane

There total 8 articles about 1-(4-bromobenzyloxy)octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: S-methyl O-[8-(4-bromobenzyloxy)oct-2-yl] carbonodithioate

: 1410119-96-8
1-(4-bromobenzyloxy)octane

Guidance literature:: With tris-(trimethylsilyl)silane; chlorophyll a; In dimethyl sulfoxide; at 50 ℃; for 5h; Reagent/catalyst; Irradiation;
DOI:10.1246/BCSJ.20200087

Reference yield:

: 111-87-5
octanol

: 589-15-1
1-bromomethyl-4-bromobenzene

: 1410119-96-8
1-(4-bromobenzyloxy)octane

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1039/c4gc00005f

Reference yield:

: 629-30-1
1,7-heptandiol

: 1410119-96-8
1-(4-bromobenzyloxy)octane

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 8 h / 20 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 - 0 °C / Inert atmosphere

3.1: oxalyl dichloride; dimethyl sulfoxide / diethyl ether / 1 h / 0 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 16 h / 0 - 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 - 20 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 13 h / 0 - 20 °C / Inert atmosphere

7.1: chlorophyll a; tris-(trimethylsilyl)silane / dimethyl sulfoxide / 5 h / 50 °C / Irradiation

With oxalyl dichloride; tris-(trimethylsilyl)silane; chlorophyll a; tetrabutyl ammonium fluoride; sodium hydride; dimethyl sulfoxide; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; 7.1: |Barton-McCombie Deoxygenation;
DOI:10.1246/BCSJ.20200087