Benzene, 1-broMo-4-[(4-Methylphenyl)Methyl]-

Base Information

Chemical Name:Benzene, 1-broMo-4-[(4-Methylphenyl)Methyl]-
CAS No.:17100-53-7
Molecular Formula:C14H13Br
Molecular Weight:261.161
Hs Code.:
Mol file:17100-53-7.mol

Synonyms:Benzene, 1-broMo-4-[(4-Methylphenyl)Methyl]-

Suppliers and Price of Benzene, 1-broMo-4-[(4-Methylphenyl)Methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 7 raw suppliers

Chemical Property of Benzene, 1-broMo-4-[(4-Methylphenyl)Methyl]-

Chemical Property:

PSA：0.00000
LogP:4.34830

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzene, 1-broMo-4-[(4-Methylphenyl)Methyl]-

There total 25 articles about Benzene, 1-broMo-4-[(4-Methylphenyl)Methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 5142-75-6
tri(p-tolyl)bismuth

: 589-17-3
p-bromobenzyl chloride

: 17100-53-7
1-bromo-4-(4-methylbenzyl)benzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 2h; chemoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1039/c3ra46672h

Reference yield: 84.0%

: 5467-74-3
4-Bromophenylboronic acid

: 104-81-4
4-Methylbenzyl bromide

: 17100-53-7
1-bromo-4-(4-methylbenzyl)benzene

Guidance literature:: 4-Methylbenzyl bromide; With lithium tert-butoxide; Schlenk technique; Inert atmosphere;

4-Bromophenylboronic acid; With α,α,α-trifluorotoluene; at 100 ℃; for 24h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.tet.2016.10.031

Reference yield: 83.0%

: 5720-05-8
4-methylphenylboronic acid

: 589-15-1
1-bromomethyl-4-bromobenzene

: 17100-53-7
1-bromo-4-(4-methylbenzyl)benzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; toluene; at 80 ℃; for 15h;
DOI:10.1016/j.tetlet.2003.10.080