(2R)-2-(benzoyl(methoxycarbonyl)carbamoyl)-3-(2-methylallyl)cyclohex-1-enylbenzoate

Base Information

Chemical Name:(2R)-2-(benzoyl(methoxycarbonyl)carbamoyl)-3-(2-methylallyl)cyclohex-1-enylbenzoate
CAS No.:1421739-35-6
Molecular Formula:C₂₇H₂₇NO₆
Molecular Weight:461.514
Hs Code.:

Synonyms:(2R)-2-(benzoyl(methoxycarbonyl)carbamoyl)-3-(2-methylallyl)cyclohex-1-enylbenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-2-(benzoyl(methoxycarbonyl)carbamoyl)-3-(2-methylallyl)cyclohex-1-enylbenzoate

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Technology Process of (2R)-2-(benzoyl(methoxycarbonyl)carbamoyl)-3-(2-methylallyl)cyclohex-1-enylbenzoate

There total 3 articles about (2R)-2-(benzoyl(methoxycarbonyl)carbamoyl)-3-(2-methylallyl)cyclohex-1-enylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1421739-29-8
(1R,2R)-methyl 4-(2-methylallyl)-2-oxo-tetrahydro-2H-pyran-3-carbonylcarbamate

: 98-88-4
benzoyl chloride

: 1421739-35-6
(2R)-2-(benzoyl(methoxycarbonyl)carbamoyl)-3-(2-methylallyl)cyclohex-1-enylbenzoate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1021/ol303381c

Reference yield:

: 1421739-42-5
methyl 6-oxocyclohex-1-enecarbonylcarbamate

: 1421739-35-6
(2R)-2-(benzoyl(methoxycarbonyl)carbamoyl)-3-(2-methylallyl)cyclohex-1-enylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: C₁₇H₂₈CuF₆N₄O₁₂S₄ / dichloromethane / 0.08 h / 20 °C / Inert atmosphere

1.2: 10.5 h / -30 °C / Inert atmosphere

2.1: triethylamine; dmap / dichloromethane / 0 °C / Inert atmosphere

With dmap; C₁₇H₂₈CuF₆N₄O₁₂S₄; triethylamine; In dichloromethane; 1.2: |Hosomi-Sakurai Reaction;
DOI:10.1021/ol303381c

Reference yield:

: C₁₀H₁₃NO₄

: 1421739-35-6
(2R)-2-(benzoyl(methoxycarbonyl)carbamoyl)-3-(2-methylallyl)cyclohex-1-enylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloro-trimethyl-silane; sodium iodide / acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere

2.1: C₁₇H₂₈CuF₆N₄O₁₂S₄ / dichloromethane / 0.08 h / 20 °C / Inert atmosphere

2.2: 10.5 h / -30 °C / Inert atmosphere

3.1: triethylamine; dmap / dichloromethane / 0 °C / Inert atmosphere

With dmap; chloro-trimethyl-silane; C₁₇H₂₈CuF₆N₄O₁₂S₄; triethylamine; sodium iodide; In dichloromethane; acetonitrile; 2.2: |Hosomi-Sakurai Reaction;
DOI:10.1021/ol303381c