1,3,5-tris<4-(((2,2'-bipyridyl-5-yl)carbonyl)benzylamino)methyl>benzene

Base Information

Chemical Name:1,3,5-tris<4-(((2,2'-bipyridyl-5-yl)carbonyl)benzylamino)methyl>benzene
CAS No.:147323-44-2
Molecular Formula:C₆₃H₅₁N₉O₃
Molecular Weight:982.156
Hs Code.:

Synonyms:1,3,5-tris<4-(((2,2'-bipyridyl-5-yl)carbonyl)benzylamino)methyl>benzene

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Chemical Property of 1,3,5-tris<4-(((2,2'-bipyridyl-5-yl)carbonyl)benzylamino)methyl>benzene

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Technology Process of 1,3,5-tris<4-(((2,2'-bipyridyl-5-yl)carbonyl)benzylamino)methyl>benzene

There total 4 articles about 1,3,5-tris<4-(((2,2'-bipyridyl-5-yl)carbonyl)benzylamino)methyl>benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.7%

: 105501-71-1
1,3,5-trisbenzene

: 140447-00-3
2,2'-bipyridine-5-carbonyl chloride

: 147323-44-2
1,3,5-tris<4-(((2,2'-bipyridyl-5-yl)carbonyl)benzylamino)methyl>benzene

Guidance literature:: With triethylamine; In N,N-dimethyl acetamide; 120 deg C;

Reference yield:

: 26482-00-8
1-(2-oxo-2-(2-pyridyl)ethyl)pyridinium iodide

: 147323-44-2
1,3,5-tris<4-(((2,2'-bipyridyl-5-yl)carbonyl)benzylamino)methyl>benzene

Guidance literature:: Multi-step reaction with 4 steps

1: NH₄OOCCH₃ / formamide

2: KMnO₄ / H₂O

3: SOCl₂ / Heating

4: 75.7 percent / triethylamine / N,N-dimethyl-acetamide / 120 deg C

With potassium permanganate; thionyl chloride; ammonium acetate; triethylamine; In N,N-dimethyl acetamide; water; formamide;

Reference yield:

: 56100-20-0
5-methyl-2,2'-bipyridine

: 147323-44-2
1,3,5-tris<4-(((2,2'-bipyridyl-5-yl)carbonyl)benzylamino)methyl>benzene

Guidance literature:: Multi-step reaction with 3 steps

1: KMnO₄ / H₂O

2: SOCl₂ / Heating

3: 75.7 percent / triethylamine / N,N-dimethyl-acetamide / 120 deg C

With potassium permanganate; thionyl chloride; triethylamine; In N,N-dimethyl acetamide; water;