exo-6-benzyl-2-m-methoxyphenyl-1-dimethylaminomethylbicyclo<2.2.2>-2-octane

Base Information

Chemical Name:exo-6-benzyl-2-m-methoxyphenyl-1-dimethylaminomethylbicyclo<2.2.2>-2-octane
CAS No.:105831-88-7
Molecular Formula:C₂₅H₃₁NO
Molecular Weight:361.527
Hs Code.:

Synonyms:exo-6-benzyl-2-m-methoxyphenyl-1-dimethylaminomethylbicyclo<2.2.2>-2-octane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of exo-6-benzyl-2-m-methoxyphenyl-1-dimethylaminomethylbicyclo<2.2.2>-2-octane

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Technology Process of exo-6-benzyl-2-m-methoxyphenyl-1-dimethylaminomethylbicyclo<2.2.2>-2-octane

There total 4 articles about exo-6-benzyl-2-m-methoxyphenyl-1-dimethylaminomethylbicyclo<2.2.2>-2-octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 105831-87-6,105881-51-4
endo- and exo-6-benzyl-2-(m-methoxyphenyl)-2-hydroxy-1-dimethylaminomethylbicyclo<2.2.2>-2-octane

: 105831-88-7
exo-6-benzyl-2-m-methoxyphenyl-1-dimethylaminomethylbicyclo<2.2.2>-2-octane

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 2h; Heating;

Reference yield:

: 36282-40-3
(3-methoxyphenyl)magnesium bromide

: 105831-88-7
exo-6-benzyl-2-m-methoxyphenyl-1-dimethylaminomethylbicyclo<2.2.2>-2-octane

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / tetrahydrofuran / 0.5 h / Ambient temperature

2: 100 percent / p-toluenesulfonic acid / benzene / 2 h / Heating

With toluene-4-sulfonic acid; In tetrahydrofuran; benzene;

Reference yield:

: 105831-83-2
exo-6-benzyl-2-hydroxy-1-dimethylaminomethylbicyclo<2.2.2>-2-octane

: 105831-88-7
exo-6-benzyl-2-m-methoxyphenyl-1-dimethylaminomethylbicyclo<2.2.2>-2-octane

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / 1.1M Jones reagent / acetone / 4 h / 0 °C

2: 59 percent / tetrahydrofuran / 0.5 h / Ambient temperature

3: 100 percent / p-toluenesulfonic acid / benzene / 2 h / Heating

With jones reagent; toluene-4-sulfonic acid; In tetrahydrofuran; acetone; benzene;