[1-((4-(adamantyl)-1H-1,2,3-triazolyl)methylene)-3-mesitylimidazolium] bromide

Base Information

• Chemical Name: [1-((4-(adamantyl)-1H-1,2,3-triazolyl)methylene)-3-mesitylimidazolium] bromide
• CAS No.: 1235962-15-8
• Molecular Formula: Br*C₂₅H₃₂N₅
• Molecular Weight: 482.467

Synonyms:[1-((4-(adamantyl)-1H-1,2,3-triazolyl)methylene)-3-mesitylimidazolium] bromide

Chemical Property of [1-((4-(adamantyl)-1H-1,2,3-triazolyl)methylene)-3-mesitylimidazolium] bromide

Chemical Property:

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Technology Process of [1-((4-(adamantyl)-1H-1,2,3-triazolyl)methylene)-3-mesitylimidazolium] bromide

There total 1 articles about [1-((4-(adamantyl)-1H-1,2,3-triazolyl)methylene)-3-mesitylimidazolium] bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1-Azidoadamantane (24886-73-5) + 1-mesityl-3-(prop-2-yn-1-yl)-1H-imidazol-3-ium bromide (960205-03-2) → [1-((4-(adamantyl)-1H-1,2,3-triazolyl)methylene)-3-mesitylimidazolium] bromide (1235962-15-8)

Guidance literature:

1-mesityl-3-(prop-2-yn-1-yl)-1H-imidazol-3-ium bromide; With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In acetonitrile; at 60 ℃; for 1h;

1-Azidoadamantane; In acetonitrile; at 60 ℃; for 48h;

DOI:10.1021/om100435x

Reference yield:

[1-((4-(adamantyl)-1H-1,2,3-triazolyl)methylene)-3-mesitylimidazolium] bromide (1235962-15-8) + silver(l) oxide (20667-12-3) → [1-((4-(adamantyl)-1H-1,2,3-triazolyl)methylene)-3-mesitylimidazol-2-ylidene]AgBr

Guidance literature:

In not given; (N2); not isolated, detected by NMR;

DOI:10.1021/om100435x

upstream raw materials:

1-Azidoadamantane

1-mesityl-3-(prop-2-yn-1-yl)-1H-imidazol-3-ium bromide

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