methyl 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-5-carboxy-v-triazole-4-carboxylate

Base Information

Chemical Name:methyl 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-5-carboxy-v-triazole-4-carboxylate
CAS No.:76143-51-6
Molecular Formula:C₃₁H₂₅N₃O₁₁
Molecular Weight:615.553
Hs Code.:

Synonyms:methyl 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-5-carboxy-v-triazole-4-carboxylate

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Chemical Property of methyl 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-5-carboxy-v-triazole-4-carboxylate

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Technology Process of methyl 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-5-carboxy-v-triazole-4-carboxylate

There total 4 articles about methyl 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-5-carboxy-v-triazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 76143-39-0
methyl 5-hydroxymethyl-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-v-triazole-4-carboxylate

: 76143-51-6
methyl 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-5-carboxy-v-triazole-4-carboxylate

Guidance literature:: With jones reagent; In acetone; at 0 ℃; for 1h;
DOI:10.1139/v80-407

Reference yield:

: 31555-05-2
methyl 4-hydroxy-2-butynoate

: 76143-51-6
methyl 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-5-carboxy-v-triazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 75.1 percent / toluene / 1.) 50 - 55 deg C, 5 d, 2.) 70 deg C, 2 d

2: 87 percent / Jones reagent / acetone / 1 h / 0 °C

With jones reagent; In acetone; toluene;
DOI:10.1139/v80-407

Reference yield:

: 69511-49-5
methyl 4-tetrahydropyranyloxy-2-butinoate

: 76143-51-6
methyl 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-5-carboxy-v-triazole-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: methanol, Dowex 50 (1+) form> / 1.5 h / 25 °C

2: 75.1 percent / toluene / 1.) 50 - 55 deg C, 5 d, 2.) 70 deg C, 2 d

3: 87 percent / Jones reagent / acetone / 1 h / 0 °C

With methanol; jones reagent; Dowex 50 ; In acetone; toluene;
DOI:10.1139/v80-407