C₁₄H₁₇N₃O

Base Information

Chemical Name:C₁₄H₁₇N₃O
CAS No.:1300556-02-8
Molecular Formula:C₁₄H₁₇N₃O
Molecular Weight:243.308
Hs Code.:

C<sub>14</sub>H<sub>17</sub>N<sub>3</sub>O

Synonyms:C₁₄H₁₇N₃O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₇N₃O

Chemical Property:

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Technology Process of C₁₄H₁₇N₃O

There total 1 articles about C₁₄H₁₇N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 51-67-2
tyrosamine

: 107-13-1,25014-41-9
acrylonitrile

: 1300556-02-8
C₁₄H₁₇N₃O

Guidance literature:: With acetic acid; for 24h; Reflux;
DOI:10.1016/j.tet.2013.01.070

Reference yield: 95.0%

: 1300556-02-8
C₁₄H₁₇N₃O

: 532381-67-2
C₁₄H₂₅N₃O

Guidance literature:: With dimethylsulfide borane complex; In tetrahydrofuran; at 20 - 26 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2013.01.070

Reference yield:

: 1300556-02-8
C₁₄H₁₇N₃O

: 1426289-99-7
C₆₈H₁₀₅N₁₅O₇S

Guidance literature:: Multi-step reaction with 5 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 20 - 26 °C / Inert atmosphere

2.1: acetic acid / 48 h / Reflux

3.1: dimethylsulfide borane complex / tetrahydrofuran / 20 - 26 °C / Inert atmosphere

4.1: methanol / 48 h / Reflux

5.1: sodium hydride / tetrahydrofuran; mineral oil / 20 - 26 °C / Inert atmosphere

5.2: 48 h / 20 - 26 °C / Inert atmosphere

With dimethylsulfide borane complex; sodium hydride; acetic acid; In tetrahydrofuran; methanol; mineral oil; 2.1: |Michael Addition / 4.1: |Michael Addition;
DOI:10.1016/j.tet.2013.01.070