1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(tert-butoxy-carbonyl-methyl)-1,4,7,10-tetraaza-cyclododecane

Base Information

Chemical Name:1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(tert-butoxy-carbonyl-methyl)-1,4,7,10-tetraaza-cyclododecane
CAS No.:1393712-12-3
Molecular Formula:C₄₃H₆₃N₇O₉S
Molecular Weight:854.081
Hs Code.:

Synonyms:1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(tert-butoxy-carbonyl-methyl)-1,4,7,10-tetraaza-cyclododecane

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Chemical Property of 1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(tert-butoxy-carbonyl-methyl)-1,4,7,10-tetraaza-cyclododecane

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Technology Process of 1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(tert-butoxy-carbonyl-methyl)-1,4,7,10-tetraaza-cyclododecane

There total 2 articles about 1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(tert-butoxy-carbonyl-methyl)-1,4,7,10-tetraaza-cyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1393712-09-8
N-(quinolin-8-yl)-2-(2-chloroacetyl)-amino-benzenesulfonamide

: 122555-91-3
1,4,7-tris-tert-butoxycarbonylmethyl-1,4,7,10-tetraazacyclododecane

: 1393712-12-3
1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(tert-butoxy-carbonyl-methyl)-1,4,7,10-tetraaza-cyclododecane

Guidance literature:: With potassium carbonate; In acetonitrile; at 70 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ic301308z

Reference yield:

: 16082-64-7
CU-242

: 1393712-12-3
1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(tert-butoxy-carbonyl-methyl)-1,4,7,10-tetraaza-cyclododecane

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 4 h / 20 °C / Inert atmosphere; Schlenk technique

2: potassium carbonate / acetonitrile / 24 h / 70 °C / Inert atmosphere; Schlenk technique

With potassium carbonate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/ic301308z

Reference yield: 92.0%

: 1393712-12-3
1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(tert-butoxy-carbonyl-methyl)-1,4,7,10-tetraaza-cyclododecane

: 1393712-14-5
1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(acetic acid)-1,4,7,10-tetraaza-cyclododecane

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ic301308z