1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(acetic acid)-1,4,7,10-tetraaza-cyclododecane

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Chemical Name:1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(acetic acid)-1,4,7,10-tetraaza-cyclododecane
CAS No.:1393712-14-5
Molecular Formula:C₃₁H₃₉N₇O₉S
Molecular Weight:685.758
Hs Code.:

Synonyms:1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(acetic acid)-1,4,7,10-tetraaza-cyclododecane

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Chemical Property of 1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(acetic acid)-1,4,7,10-tetraaza-cyclododecane

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Technology Process of 1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(acetic acid)-1,4,7,10-tetraaza-cyclododecane

There total 2 articles about 1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(acetic acid)-1,4,7,10-tetraaza-cyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1393712-12-3
1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(tert-butoxy-carbonyl-methyl)-1,4,7,10-tetraaza-cyclododecane

: 1393712-14-5
1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(acetic acid)-1,4,7,10-tetraaza-cyclododecane

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ic301308z

Reference yield:

: 16082-64-7
CU-242

: 1393712-14-5
1-(2-N-quinolin-8-yl-benzenesulfonamino-acetamide)-4,7,10-tris(acetic acid)-1,4,7,10-tetraaza-cyclododecane

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 4 h / 20 °C / Inert atmosphere; Schlenk technique

2: potassium carbonate / acetonitrile / 24 h / 70 °C / Inert atmosphere; Schlenk technique

3: trifluoroacetic acid / dichloromethane / 24 h / 20 °C / Inert atmosphere; Schlenk technique

With potassium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1021/ic301308z