all-(E)-5-methoxy-2-(14'-phenyltetradeca-7',9',11',13'-tetraenyl)-[1,3]dioxane

Base Information

Chemical Name:all-(E)-5-methoxy-2-(14'-phenyltetradeca-7',9',11',13'-tetraenyl)-[1,3]dioxane
CAS No.:792923-45-6
Molecular Formula:C₂₅H₃₄O₃
Molecular Weight:382.543
Hs Code.:

Synonyms:all-(E)-5-methoxy-2-(14'-phenyltetradeca-7',9',11',13'-tetraenyl)-[1,3]dioxane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of all-(E)-5-methoxy-2-(14'-phenyltetradeca-7',9',11',13'-tetraenyl)-[1,3]dioxane

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Technology Process of all-(E)-5-methoxy-2-(14'-phenyltetradeca-7',9',11',13'-tetraenyl)-[1,3]dioxane

There total 1 articles about all-(E)-5-methoxy-2-(14'-phenyltetradeca-7',9',11',13'-tetraenyl)-[1,3]dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 5-methoxy-2-(14'-phenyltetradeca-9',11',13'-trien-7'-ynyl)-[1,3]dioxane

: 792923-45-6
all-(E)-5-methoxy-2-(14'-phenyltetradeca-7',9',11',13'-tetraenyl)-[1,3]dioxane

Guidance literature:: 5-methoxy-2-(14'-phenyltetradeca-9',11',13'-trien-7'-ynyl)-[1,3]dioxane; With copper diacetate; silver nitrate; zinc; In methanol; ethanol; at 20 ℃; for 17h;

With iodine; In hexane; for 0.25h; Heating;
DOI:10.1021/jm049808a

Reference yield:

: 792923-45-6
all-(E)-5-methoxy-2-(14'-phenyltetradeca-7',9',11',13'-tetraenyl)-[1,3]dioxane

: 791845-23-3
all-(E)-2-methoxy-3-(15'-phenylpentadeca-8',10',12',14'-tetraenyloxy)propan-1-ol

Guidance literature:: With diisobutylaluminium hydride; In toluene; at 20 ℃; for 4h;
DOI:10.1021/jm049808a

Reference yield:

: 792923-45-6
all-(E)-5-methoxy-2-(14'-phenyltetradeca-7',9',11',13'-tetraenyl)-[1,3]dioxane

: all-(E)-1-O-(15'-phenylpentadeca-8',10',12',14'-tetraenyl)-2-O-methyl-rac-glycero-3-phosphocholine

Guidance literature:: Multi-step reaction with 2 steps

1: DIBAL-H / toluene / 4 h / 20 °C

2: acetonitrile / 3 h / 20 - 70 °C

With diisobutylaluminium hydride; In toluene; acetonitrile;
DOI:10.1021/jm049808a