C₃₃H₄₁N₅O₂

Base Information

Chemical Name:C₃₃H₄₁N₅O₂
CAS No.:1430093-77-8
Molecular Formula:C₃₃H₄₁N₅O₂
Molecular Weight:539.721
Hs Code.:

C<sub>33</sub>H<sub>41</sub>N<sub>5</sub>O<sub>2</sub>

Synonyms:C₃₃H₄₁N₅O₂

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Chemical Property of C₃₃H₄₁N₅O₂

Chemical Property:

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Technology Process of C₃₃H₄₁N₅O₂

There total 11 articles about C₃₃H₄₁N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1430093-76-7
C₃₈H₄₉N₅O₄

: 1430093-77-8
C₃₃H₄₁N₅O₂

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.3762/bjoc.9.31

Reference yield:

: 1430093-64-3
C₁₅H₁₉FN₂O₆

: 1430093-77-8
C₃₃H₄₁N₅O₂

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

2: hydrogen; palladium 10% on activated carbon / methanol / 20 °C / 760.05 Torr

3: potassium peroxymonosulfate / N,N-dimethyl-formamide; water / 24 h / 20 °C / Inert atmosphere

4: lithium hydroxide; water / methanol; tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5: triethylamine / tetrahydrofuran / 1 h / -42 °C / Inert atmosphere

6: ammonia / tetrahydrofuran / -42 - 20 °C / Inert atmosphere

7: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With potassium peroxymonosulfate; palladium 10% on activated carbon; ammonia; water; hydrogen; potassium carbonate; triethylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.3762/bjoc.9.31

Reference yield:

: 1430093-71-2
C₁₀H₁₁FN₂O₄

: 1430093-77-8
C₃₃H₄₁N₅O₂

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / water; tetrahydrofuran; 1,4-dioxane / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

3: hydrogen; palladium 10% on activated carbon / methanol / 20 °C / 760.05 Torr

4: potassium peroxymonosulfate / N,N-dimethyl-formamide; water / 24 h / 20 °C / Inert atmosphere

5: lithium hydroxide; water / methanol; tetrahydrofuran / 0 - 20 °C / Inert atmosphere

6: triethylamine / tetrahydrofuran / 1 h / -42 °C / Inert atmosphere

7: ammonia / tetrahydrofuran / -42 - 20 °C / Inert atmosphere

8: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With potassium peroxymonosulfate; palladium 10% on activated carbon; ammonia; water; hydrogen; potassium carbonate; triethylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.3762/bjoc.9.31