benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-L-glycero-α-D-mannoheptopyranoside

Base Information

Chemical Name:benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-L-glycero-α-D-mannoheptopyranoside
CAS No.:1554004-95-3
Molecular Formula:C₅₆H₅₇O₁₀P
Molecular Weight:921.036
Hs Code.:

Synonyms:benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-L-glycero-α-D-mannoheptopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-L-glycero-α-D-mannoheptopyranoside

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Technology Process of benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-L-glycero-α-D-mannoheptopyranoside

There total 4 articles about benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-L-glycero-α-D-mannoheptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₆H₅₇O₉P

: 1554004-95-3
benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-L-glycero-α-D-mannoheptopyranoside

Guidance literature:: With tert.-butylhydroperoxide; In decane; at -20 - 20 ℃;
DOI:10.1016/j.bmc.2013.12.019

Reference yield:

: 732296-48-9
benzyl 7-O-tetra-butyldiphenylsilyl-2,3,4,6-O-tetra-benzyl-L-glycero-α-D-mannoheptopyranoside

: 1554004-95-3
benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-L-glycero-α-D-mannoheptopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

2.1: 1H-tetrazole / dichloromethane; acetonitrile / 0.5 h / 20 °C / Molecular sieve

2.2: 2 h / 20 °C

3.1: tert.-butylhydroperoxide / decane / -20 - 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; tetrabutyl ammonium fluoride; In tetrahydrofuran; decane; dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2013.12.019

Reference yield:

: 100-39-0
benzyl bromide

: 1554004-95-3
benzyl 7-O-dibenzyl-phosphono-2,3,4,6-O-tetra-benzyl-L-glycero-α-D-mannoheptopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride; tetra-(n-butyl)ammonium iodide / mineral oil; tetrahydrofuran / 0 - 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

3.1: 1H-tetrazole / dichloromethane; acetonitrile / 0.5 h / 20 °C / Molecular sieve

3.2: 2 h / 20 °C

4.1: tert.-butylhydroperoxide / decane / -20 - 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; decane; dichloromethane; acetonitrile; mineral oil;
DOI:10.1016/j.bmc.2013.12.019