Acetic acid 2-tert-butyl-4-nitro-6-{[(pyridin-2-ylmethyl)-amino]-methyl}-phenyl ester

Base Information

Chemical Name:Acetic acid 2-tert-butyl-4-nitro-6-{[(pyridin-2-ylmethyl)-amino]-methyl}-phenyl ester
CAS No.:205313-84-4
Molecular Formula:C₁₉H₂₃N₃O₄
Molecular Weight:357.409
Hs Code.:

Synonyms:Acetic acid 2-tert-butyl-4-nitro-6-{[(pyridin-2-ylmethyl)-amino]-methyl}-phenyl ester

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Chemical Property of Acetic acid 2-tert-butyl-4-nitro-6-{[(pyridin-2-ylmethyl)-amino]-methyl}-phenyl ester

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Technology Process of Acetic acid 2-tert-butyl-4-nitro-6-{[(pyridin-2-ylmethyl)-amino]-methyl}-phenyl ester

There total 4 articles about Acetic acid 2-tert-butyl-4-nitro-6-{[(pyridin-2-ylmethyl)-amino]-methyl}-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 3731-51-9
2-(Aminomethyl)pyridine

: 205313-83-3
2-bromomethyl-6-tert-butyl-4-nitrophenyl acetate

: 205313-84-4
Acetic acid 2-tert-butyl-4-nitro-6-{[(pyridin-2-ylmethyl)-amino]-methyl}-phenyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; for 15h; Heating;

Reference yield:

: 2219-82-1
2-tert-Butyl-6-methylphenol

: 205313-84-4
Acetic acid 2-tert-butyl-4-nitro-6-{[(pyridin-2-ylmethyl)-amino]-methyl}-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / HNO₃ (65percent) / CH₂Cl₂ / 0 °C

2: 85 percent / triethylamine / CH₂Cl₂ / Heating

3: 56 percent / NBS, traces of benzoyl peroxide / CCl₄ / 38 h / Heating

4: 96 percent / triethylamine / tetrahydrofuran / 15 h / Heating

With N-Bromosuccinimide; Perbenzoic acid; nitric acid; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane;

Reference yield:

: 10396-84-6
2-tert-butyl-4-nitro-6-methylphenol

: 205313-84-4
Acetic acid 2-tert-butyl-4-nitro-6-{[(pyridin-2-ylmethyl)-amino]-methyl}-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / triethylamine / CH₂Cl₂ / Heating

2: 56 percent / NBS, traces of benzoyl peroxide / CCl₄ / 38 h / Heating

3: 96 percent / triethylamine / tetrahydrofuran / 15 h / Heating

With N-Bromosuccinimide; Perbenzoic acid; triethylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane;