phenyl-carbamic acid 7-oxo-heptyl ester

Base Information

Chemical Name:phenyl-carbamic acid 7-oxo-heptyl ester
CAS No.:547740-47-6
Molecular Formula:C₁₄H₁₉NO₃
Molecular Weight:249.31
Hs Code.:

Synonyms:phenyl-carbamic acid 7-oxo-heptyl ester

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Chemical Property of phenyl-carbamic acid 7-oxo-heptyl ester

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Technology Process of phenyl-carbamic acid 7-oxo-heptyl ester

There total 6 articles about phenyl-carbamic acid 7-oxo-heptyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.4%

: 201230-82-2
carbon monoxide

: 547740-45-4
N-phenylcarbamic acid hex-5-enyl ester

: phenyl-carbamic acid 5-methyl-6-oxo-hexyl ester

: 547740-47-6
phenyl-carbamic acid 7-oxo-heptyl ester

Guidance literature:: With acetylacetonatodicarbonylrhodium(l); hydrogen; (2-oxo-1,2-dihydro-6-pyridyl)diphenylphosphine; In toluene; at 70 ℃; for 20h; under 7500.6 Torr;
DOI:10.1021/ja0348997

Reference yield: 83.0%

: 201230-82-2
carbon monoxide

: 547740-45-4
N-phenylcarbamic acid hex-5-enyl ester

: 547740-47-6
phenyl-carbamic acid 7-oxo-heptyl ester

Guidance literature:: With dicarbonylacetylacetonato rhodium (I); polyoxyethanyl α-tocopheryl sebacate; hydrogen; (2-oxo-1,2-dihydro-6-pyridyl)diphenylphosphine; In water; at 20 ℃; for 24h; under 760.051 Torr; regioselective reaction; Schlenk technique;
DOI:10.1002/adsc.201300258

Reference yield:

: 201230-82-2
carbon monoxide

: 547740-45-4
N-phenylcarbamic acid hex-5-enyl ester

: Phenyl-carbamic acid (E)-hex-3-enyl ester

: Phenyl-carbamic acid (E)-hex-4-enyl ester

: phenyl-carbamic acid 5-methyl-6-oxo-hexyl ester

: 547740-47-6
phenyl-carbamic acid 7-oxo-heptyl ester

Guidance literature:: With hydrogen; (2-oxo-1,2-dihydro-6-pyridyl)diphenylphosphine; acetylacetonatodicarbonylrhodium(l); In tetrahydrofuran; at 22 ℃; for 20h; under 760 Torr; Further byproducts given. Title compound not separated from byproducts;
DOI:10.1002/adsc.200505174