N,N-diethyl-2,3-dihydro-2,4-dimethyl-3-phenyl-2-azetecarboxamide 1-oxide

Base Information

• Chemical Name: N,N-diethyl-2,3-dihydro-2,4-dimethyl-3-phenyl-2-azetecarboxamide 1-oxide
• CAS No.: 75909-31-8
• Molecular Formula: C₁₆H₂₂N₂O₂
• Molecular Weight: 274.363

Synonyms:N,N-diethyl-2,3-dihydro-2,4-dimethyl-3-phenyl-2-azetecarboxamide 1-oxide

Chemical Property of N,N-diethyl-2,3-dihydro-2,4-dimethyl-3-phenyl-2-azetecarboxamide 1-oxide

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of N,N-diethyl-2,3-dihydro-2,4-dimethyl-3-phenyl-2-azetecarboxamide 1-oxide

There total 9 articles about N,N-diethyl-2,3-dihydro-2,4-dimethyl-3-phenyl-2-azetecarboxamide 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

N,N-diethyl-1-hydroxy-2,4-dimethyl-3-phenyl-2-azetinecarboxamide (82264-40-2) → N,N-diethyl-2,3-dihydro-2,4-dimethyl-3-phenyl-2-azetecarboxamide 1-oxide (75909-31-8)

Guidance literature:

With mercury(II) oxide; In dichloromethane; at 25 ℃; for 3h;

DOI:10.1021/jo00144a006

Reference yield: 76.0%

(2R,3S,4S)-1-Hydroxy-2,4-dimethyl-3-phenyl-azetidine-2-carboxylic acid diethylamide (82238-35-5,82264-40-2) → (2R,3R)-2,4-Dimethyl-1-oxy-3-phenyl-2,3-dihydro-azete-2-carboxylic acid diethylamide (73227-46-0,75909-31-8)

Guidance literature:

With mercury(II) oxide;

DOI:10.1016/S0040-4039(00)87005-7

Reference yield: 73.0%

(2α,3α,4α)-N,N-diethyl-1-hydroxy-2,4-dimethyl-3-phenyl-2-azetidinecarboxamide (82238-35-5) → N,N-diethyl-2,3-dihydro-2,4-dimethyl-3-phenyl-2-azetecarboxamide 1-oxide (75909-31-8)

Guidance literature:

With mercury(II) oxide; In dichloromethane; at 25 ℃; for 5h;

DOI:10.1021/jo00144a006

upstream raw materials:

(2R,3S,4S)-1-Hydroxy-2,4-dimethyl-3-phenyl-azetidine-2-carboxylic acid diethylamide

(2R,3S,4R)-1-Hydroxy-2,4-dimethyl-3-phenyl-azetidine-2-carboxylic acid diethylamide

(2α,3α,4α)-N,N-diethyl-1-hydroxy-2,4-dimethyl-3-phenyl-2-azetidinecarboxamide

N,N-diethyl-1-hydroxy-2,4-dimethyl-3-phenyl-2-azetinecarboxamide

Downstream raw materials:

(2R,3S,4R)-1-Hydroxy-2,4-dimethyl-3-phenyl-azetidine-2-carboxylic acid diethylamide

N,N-diethyl-3-chloro-2-methyl-4-(2-oxopropylidene)-3-phenyl-2-azetidinecarboxamide

N,N-diethyl-2-<(acetyloxy)amino>-2-methyl-4-oxo-3-phenylpentanamide

(2α,3α,4α)-N,N-diethyl-1-hydroxy-2,4-dimethyl-3-phenyl-2-azetidinemethanamine

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