3-allyl-6-bromo-7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Base Information

Chemical Name:3-allyl-6-bromo-7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine
CAS No.:135974-56-0
Molecular Formula:C₂₁H₂₄BrNO₂
Molecular Weight:402.331
Hs Code.:

Synonyms:3-allyl-6-bromo-7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-allyl-6-bromo-7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

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Technology Process of 3-allyl-6-bromo-7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

There total 3 articles about 3-allyl-6-bromo-7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 67287-40-5
6-bromo-7,8-dimethoxy-2,3,4,5-tetrahydro-1-phenyl-1H-3-benzazepine hydrobromide

: 106-95-6
allyl bromide

: 135974-56-0
3-allyl-6-bromo-7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1021/jm00116a004

Reference yield:

: 20569-49-7
7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

: 135974-56-0
3-allyl-6-bromo-7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / glacial acetic acid, bromine / 2 h / Ambient temperature

2: 60 percent / K₂CO₃ / dimethylformamide / Ambient temperature

With bromine; potassium carbonate; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm00116a004

Reference yield:

: 20011-97-6
N-[2-(3,4-dimethoxyphenyl)ethyl]-2-phenyl-2-hydroxyethylamine

: 135974-56-0
3-allyl-6-bromo-7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / trifluoroacetic acid, H₂SO₄ / 3 h / Heating

2: 69 percent / glacial acetic acid, bromine / 2 h / Ambient temperature

3: 60 percent / K₂CO₃ / dimethylformamide / Ambient temperature

With sulfuric acid; bromine; potassium carbonate; acetic acid; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm00116a004