2-Phenyl-1,3-dioxane-5-yl-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxy>carbonic acid ester

Base Information

Chemical Name:2-Phenyl-1,3-dioxane-5-yl-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxy>carbonic acid ester
CAS No.:150995-00-9
Molecular Formula:C₂₇H₂₄N₂O₆
Molecular Weight:472.497
Hs Code.:

Synonyms:2-Phenyl-1,3-dioxane-5-yl-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxy>carbonic acid ester

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Chemical Property of 2-Phenyl-1,3-dioxane-5-yl-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxy>carbonic acid ester

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Technology Process of 2-Phenyl-1,3-dioxane-5-yl-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxy>carbonic acid ester

There total 3 articles about 2-Phenyl-1,3-dioxane-5-yl-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxy>carbonic acid ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 150994-99-3
cis/trans-2-phenyl-5-carboxy-1,3-dioxane

: 21616-46-6
3-hydroxymethyl-5,5-diphenyl-imidazolidine-2,4-dione

: 150995-00-9
2-Phenyl-1,3-dioxane-5-yl-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxy>carbonic acid ester

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1002/ardp.19933260810

Reference yield:

: 100-52-7
benzaldehyde

: 150995-00-9
2-Phenyl-1,3-dioxane-5-yl-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxy>carbonic acid ester

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / p-TsOH / toluene / Heating

2: 1) KOH, 2) pyridine / 1) EtOH, 2 h, reflux, 2) 3 h, reflux

3: 91 percent / Et₃N, bis(2-oxo-3-oxazolidinyl)phosphinic acid chloride / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; potassium hydroxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; toluene-4-sulfonic acid; triethylamine; In dichloromethane; toluene;
DOI:10.1002/ardp.19933260810

Reference yield:

: 71348-41-9
diethyl 6-phenyl-[1,5]-dioxane-3,3-dicarboxylic acid diester

: 150995-00-9
2-Phenyl-1,3-dioxane-5-yl-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxy>carbonic acid ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) KOH, 2) pyridine / 1) EtOH, 2 h, reflux, 2) 3 h, reflux

2: 91 percent / Et₃N, bis(2-oxo-3-oxazolidinyl)phosphinic acid chloride / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; potassium hydroxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In dichloromethane;
DOI:10.1002/ardp.19933260810