1-<<3-ethyl-2-<(3-methyl-2-butenyl)oxy>-2-pentenyl>sulfonyl>-4-methylbenzene

Base Information

• Chemical Name: 1-<<3-ethyl-2-<(3-methyl-2-butenyl)oxy>-2-pentenyl>sulfonyl>-4-methylbenzene
• CAS No.: 109787-64-6
• Molecular Formula: C₁₉H₂₈O₃S
• Molecular Weight: 336.496

Synonyms:1-<<3-ethyl-2-<(3-methyl-2-butenyl)oxy>-2-pentenyl>sulfonyl>-4-methylbenzene

Chemical Property of 1-<<3-ethyl-2-<(3-methyl-2-butenyl)oxy>-2-pentenyl>sulfonyl>-4-methylbenzene

Chemical Property:

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Technology Process of 1-<<3-ethyl-2-<(3-methyl-2-butenyl)oxy>-2-pentenyl>sulfonyl>-4-methylbenzene

There total 4 articles about 1-<<3-ethyl-2-<(3-methyl-2-butenyl)oxy>-2-pentenyl>sulfonyl>-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1-<<3-ethyl-1,2-pentadienyl>sulfonyl>-4-methylbenzene (109787-30-6) + 3-methyl-2-buten-1-ol (556-82-1) → 1-<<3-ethyl-2-<(3-methyl-2-butenyl)oxy>-2-pentenyl>sulfonyl>-4-methylbenzene (109787-64-6)

Guidance literature:

With potassium hydride; In tetrahydrofuran; for 0.166667h; Ambient temperature;

DOI:10.1021/jo00227a017

Reference yield:

4-methylbenzenesulfinyl chloride (10439-23-3) → 1-<<3-ethyl-2-<(3-methyl-2-butenyl)oxy>-2-pentenyl>sulfonyl>-4-methylbenzene (109787-64-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 84 percent / pyridine / 0.75 h / Ambient temperature

2: 98 percent / CCl₄ / 13.5 h / Heating

3: 80 percent / KH / tetrahydrofuran / 0.17 h / Ambient temperature

With pyridine; potassium hydride; In tetrahydrofuran; tetrachloromethane;

DOI:10.1021/jo00227a017

Reference yield:

3-ethyl-1-pentyn-3-ol (6285-06-9) → 1-<<3-ethyl-2-<(3-methyl-2-butenyl)oxy>-2-pentenyl>sulfonyl>-4-methylbenzene (109787-64-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 84 percent / pyridine / 0.75 h / Ambient temperature

2: 98 percent / CCl₄ / 13.5 h / Heating

3: 80 percent / KH / tetrahydrofuran / 0.17 h / Ambient temperature

With pyridine; potassium hydride; In tetrahydrofuran; tetrachloromethane;

DOI:10.1021/jo00227a017

upstream raw materials:

1-<<3-ethyl-1,2-pentadienyl>sulfonyl>-4-methylbenzene

3-methyl-2-buten-1-ol

4-methylbenzenesulfinyl chloride

3-ethyl-1-pentyn-3-ol

Downstream raw materials:

3,3-Diethyl-4,4-dimethyl-1-((4-methylphenyl)sulfonyl)-5-hexene-2-one

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