Benzyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-α-D-mannopyranoside

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Chemical Name:Benzyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-α-D-mannopyranoside
CAS No.:155195-10-1
Molecular Formula:C₄₆H₆₇FO₁₇Si₂
Molecular Weight:967.197
Hs Code.:

Synonyms:Benzyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-α-D-mannopyranoside

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Chemical Property of Benzyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-α-D-mannopyranoside

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Technology Process of Benzyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-α-D-mannopyranoside

There total 3 articles about Benzyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 155194-89-1
Benzyl 2-O-benzoyl-4,6-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-mannopyranoside

: 439-03-2,439-04-3,439-05-4,2823-44-1,2823-46-3,3934-29-0,4163-44-4,4163-45-5,20409-31-8,23235-96-3,51897-75-7,51897-76-8,51897-77-9,57573-38-3,62561-28-8,126641-47-2
2,3,4,6-tetra-O-acetyl-1-fluoro-α-D-glucopyranose

: 155195-10-1
Benzyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-α-D-mannopyranoside

Guidance literature:: boron trifluoride diethyl etherate; In dichloromethane; for 24h; Ambient temperature;

Reference yield:

: 98-88-4
benzoyl chloride

: 155195-10-1
Benzyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / pyridine / 2 h / Ambient temperature

2: 85 percent / BF₃*Et₂O / CH₂Cl₂ / 24 h / Ambient temperature

With pyridine; boron trifluoride diethyl etherate; In dichloromethane;

Reference yield:

: 145259-85-4
(2S,3S,4R,4aS,10aR)-2-Benzyloxy-6,6,8,8-tetraisopropyl-hexahydro-1,5,7,9-tetraoxa-6,8-disila-benzocyclooctene-3,4-diol

: 155195-10-1
Benzyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / pyridine / 2 h / Ambient temperature

2: 85 percent / BF₃*Et₂O / CH₂Cl₂ / 24 h / Ambient temperature

With pyridine; boron trifluoride diethyl etherate; In dichloromethane;