1-(2-azido-2-deoxy-β-D-arabinofuranosyl)-5-benzylideneamino-4-cyanoimidazole

Base Information

Chemical Name:1-(2-azido-2-deoxy-β-D-arabinofuranosyl)-5-benzylideneamino-4-cyanoimidazole
CAS No.:125339-01-7
Molecular Formula:C₁₆H₁₅N₇O₃
Molecular Weight:353.34
Hs Code.:

Synonyms:1-(2-azido-2-deoxy-β-D-arabinofuranosyl)-5-benzylideneamino-4-cyanoimidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-azido-2-deoxy-β-D-arabinofuranosyl)-5-benzylideneamino-4-cyanoimidazole

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Technology Process of 1-(2-azido-2-deoxy-β-D-arabinofuranosyl)-5-benzylideneamino-4-cyanoimidazole

There total 6 articles about 1-(2-azido-2-deoxy-β-D-arabinofuranosyl)-5-benzylideneamino-4-cyanoimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 125338-99-0
1-<2-azido-2-deoxy-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-arabinofuranosyl>-5-benzylideneamino-4-cyanoimidazole

: 125339-01-7
1-(2-azido-2-deoxy-β-D-arabinofuranosyl)-5-benzylideneamino-4-cyanoimidazole

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.0833333h; Ambient temperature;
DOI:10.1248/cpb.37.1604

Reference yield:

: 100-52-7
benzaldehyde

: 125339-01-7
1-(2-azido-2-deoxy-β-D-arabinofuranosyl)-5-benzylideneamino-4-cyanoimidazole

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

2: 75 percent / 4-dimethylaminopyridine, pyridine / triethylamine / 0.5 h / Ambient temperature

3: 83 percent / NaN₃ / dimethylformamide / 24 h / Ambient temperature

4: 70 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.08 h / Ambient temperature

With pyridine; dmap; sodium azide; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; In tetrahydrofuran; triethylamine; N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.37.1604

Reference yield:

: 125338-91-2
5-amino-4-cyano-1-(3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl)imidazole

: 125339-01-7
1-(2-azido-2-deoxy-β-D-arabinofuranosyl)-5-benzylideneamino-4-cyanoimidazole

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

2: 75 percent / 4-dimethylaminopyridine, pyridine / triethylamine / 0.5 h / Ambient temperature

3: 83 percent / NaN₃ / dimethylformamide / 24 h / Ambient temperature

4: 70 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.08 h / Ambient temperature

With pyridine; dmap; sodium azide; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; In tetrahydrofuran; triethylamine; N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.37.1604