[chlororuthenium(II) bis(triphenylphosphane)(η6-p-cymene)] hexafluorophosphate

Base Information

Chemical Name:[chlororuthenium(II) bis(triphenylphosphane)(η6-p-cymene)] hexafluorophosphate
CAS No.:846550-68-3
Molecular Formula:C₄₆H₄₄ClP₂Ru*F₆P
Molecular Weight:940.29
Hs Code.:

Synonyms:[chlororuthenium(II) bis(triphenylphosphane)(η6-p-cymene)] hexafluorophosphate

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Chemical Property of [chlororuthenium(II) bis(triphenylphosphane)(η6-p-cymene)] hexafluorophosphate

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Technology Process of [chlororuthenium(II) bis(triphenylphosphane)(η6-p-cymene)] hexafluorophosphate

There total 5 articles about [chlororuthenium(II) bis(triphenylphosphane)(η6-p-cymene)] hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 923276-33-9
[Ru^II(η⁶-p-cymene)(PPh₃)(CH₃CN)Cl]PF₆

: 603-35-0
triphenylphosphine

: 846550-68-3
[chlororuthenium(II) bis(triphenylphosphane)(η6-p-cymene)] hexafluorophosphate

Guidance literature:: In dichloromethane; under N2 atm. to soln. Ru complex in CH2Cl2 PPh3 was added and stirred at room temp. for 3 h; Et2O was added, ppt. was washed with Et2O, reppn. from CH2Cl2 with pentane; elem. anal.;
DOI:10.1021/om070050d

Reference yield: 78.0%

: 17084-13-8
potassium hexafluorophosphate

: 52490-94-5
[dichloro(p-cymene)(triphenylphosphane)ruthenium(II)]

: 603-35-0
triphenylphosphine

: 846550-68-3
[chlororuthenium(II) bis(triphenylphosphane)(η6-p-cymene)] hexafluorophosphate

Guidance literature:: In methanol; at 35 ℃; for 2h;
DOI:10.1016/j.jinorgbio.2014.03.002

Reference yield: 78.0%

: ammonium hexafluorophosphate

: 52490-94-5
[dichloro(p-cymene)(triphenylphosphane)ruthenium(II)]

: 603-35-0
triphenylphosphine

: 846550-68-3
[chlororuthenium(II) bis(triphenylphosphane)(η6-p-cymene)] hexafluorophosphate

Guidance literature:: In methanol; under N2 atm. suspn. Ru complex, PPh3 and (NH4)PF6 in MeOH was stirred at 35°C for 2 h; solvent was removed in vacuo, residue was extd. with CH2Cl2 through Celite, pptn. with pentane and washing with EtOH;
DOI:10.1021/om070050d