[(2,2'-phenylphosphino)bis(4,6-di-tert-butylphenolate)]SnMe₂

Base Information

• Chemical Name: [(2,2'-phenylphosphino)bis(4,6-di-tert-butylphenolate)]SnMe₂
• CAS No.: 950733-58-1
• Molecular Formula: C₃₆H₅₁O₂PSn
• Molecular Weight: 665.483

Synonyms:[(2,2'-phenylphosphino)bis(4,6-di-tert-butylphenolate)]SnMe₂

Chemical Property of [(2,2'-phenylphosphino)bis(4,6-di-tert-butylphenolate)]SnMe₂

Chemical Property:

Purity/Quality:

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Technology Process of [(2,2'-phenylphosphino)bis(4,6-di-tert-butylphenolate)]SnMe₂

There total 1 articles about [(2,2'-phenylphosphino)bis(4,6-di-tert-butylphenolate)]SnMe₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

dimethyltin dichloride (753-73-1) + bis(3,5-di-tert-butyl-2-hydroxyphenyl)phenylphosphine → [(2,2'-phenylphosphino)bis(4,6-di-tert-butylphenolate)]SnMe2 (950733-58-1)

Guidance literature:

With n-BuLi; In tetrahydrofuran; hexane; under N2; to THF soln. of a ligand (0.39 mmol) cooled to -35°C was added dropwise a soln. of n-BuLi (0.77 mmol) in hexane; stirring at room temp. for 1 h; cooling to -35°C; prechilled soln. of Me2SnCl2 (0.39 mmol) in THF was added dropwise; after the react. mixt. was stirred at room temp. for 16 h and evapd. to dryness under reduced pressure, solid thus obtained was dissolved in pentane; soln. was filtered through a pad of Celite and evapd. to dryness; elem. anal.;

DOI:10.1021/ic701006r

upstream raw materials:

dimethyltin dichloride

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