isopropyl Methoxycinnamate

Base Information

• Chemical Name: isopropyl Methoxycinnamate
• CAS No.: 195625-04-8
• Molecular Formula: C₁₃H₁₆O₃
• Molecular Weight: 220.268
• Mol file: 195625-04-8.mol

Synonyms:isopropyl Methoxycinnamate

Chemical Property of isopropyl Methoxycinnamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of isopropyl Methoxycinnamate

There total 2 articles about isopropyl Methoxycinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-allylanisole (3698-28-0) + isopropyl alcohol (67-63-0,8013-70-5) → isopropyl Methoxycinnamate (195625-04-8)

Guidance literature:

2-allylanisole; With tris(triphenylphosphine)ruthenium(II) chloride; In dichloromethane; for 2h; Reflux;

isopropyl alcohol; With oxygen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 1h; regioselective reaction; Reflux;

DOI:10.1055/s-0032-1318146

Reference yield:

→ isopropyl Methoxycinnamate (195625-04-8)

Guidance literature:

Reference yield: 72.0%

isopropyl Methoxycinnamate (195625-04-8) + N-bromoacetamide (79-15-2) → (2R,3S)-3-Acetylamino-2-hydroxy-3-(2-methoxy-phenyl)-propionic acid isopropyl ester

Guidance literature:

With lithium hydroxide; Hydroquinone 1,4-phthalazinediyl diether; K2; In tert-butyl alcohol; at 4 ℃; for 20h;

DOI:10.1002/anie.199714831

upstream raw materials:

2-allylanisole

isopropyl alcohol