(4S)-4-benzyl-3-{(R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-pentenoyl}-2-oxazolidinone

Base Information

• Chemical Name: (4S)-4-benzyl-3-{(R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-pentenoyl}-2-oxazolidinone
• CAS No.: 865872-68-0
• Molecular Formula: C₃₀H₃₁NO₆
• Molecular Weight: 501.579

Synonyms:(4S)-4-benzyl-3-{(R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-pentenoyl}-2-oxazolidinone

Chemical Property of (4S)-4-benzyl-3-{(R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-pentenoyl}-2-oxazolidinone

Chemical Property:

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Technology Process of (4S)-4-benzyl-3-{(R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-pentenoyl}-2-oxazolidinone

There total 1 articles about (4S)-4-benzyl-3-{(R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-pentenoyl}-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-methoxy-4-(phenylmethoxy)benzaldehyde (2426-87-1) + (4S)-4-benzyl-3-pent-4-enoyl-1,3-oxazolidin-2-one (104266-88-8) → (4S)-4-benzyl-3-{(R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-pentenoyl}-2-oxazolidinone (865872-68-0)

Guidance literature:

With chloro-trimethyl-silane; triethylamine; magnesium chloride; In ethyl acetate; at 20 ℃; for 16h;

DOI:10.1271/bbb.69.113

Reference yield: 96.0%

(4S)-4-benzyl-3-{(R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-pentenoyl}-2-oxazolidinone (865872-68-0) + chloromethyl methyl ether (107-30-2) → (4S)-4-benzyl-3-{(R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(methoxymethoxy)methyl]-4-pentenoyl}-2-oxazolidinone (1204225-44-4)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1271/bbb.90167

Reference yield: 78.0%

(4S)-4-benzyl-3-{(R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-pentenoyl}-2-oxazolidinone (865872-68-0) + triisopropylsilyl trifluoromethanesulfonate (80522-42-5) → (4S)-4-benzyl-3-{(R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-pentenoyl}-2-oxazolidinone (865872-69-1)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 1.5h;

DOI:10.1271/bbb.69.113 DOI:10.1021/np050089s

upstream raw materials:

3-methoxy-4-(phenylmethoxy)benzaldehyde

(4S)-4-benzyl-3-pent-4-enoyl-1,3-oxazolidin-2-one

Downstream raw materials:

(4S)-4-benzyl-3-{(R)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-pentenoyl}-2-oxazolidinone

(3S,4S)-4-(4-benzyloxy-3-methoxyphenyl)-3-pivaloyloxymethyl-4-butanolide

2,2-dimethyl-propionic acid 2-(4-benzyloxy-3-methoxy-phenyl)-5-hydroxy-tetrahydro-furan-3-ylmethyl ester

(2S)-2-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-penten-1-ol

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