(C₁₂H₈N₂)Pd(C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)*CH₂Cl₂ = [(C₁₂H₈N₂)Pd(C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4*CH₂Cl₂

Base Information

• Chemical Name: (C₁₂H₈N₂)Pd(C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)*CH₂Cl₂ = [(C₁₂H₈N₂)Pd(C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4*CH₂Cl₂
• CAS No.: 175857-99-5
• Molecular Formula: CH₂Cl₂*C₁₅H₁₁N₂O₂Pd*C₃₂H₁₂BF₂₄
• Molecular Weight: 1305.84

Synonyms:(C₁₂H₈N₂)Pd(C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)*CH₂Cl₂ = [(C₁₂H₈N₂)Pd(C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4*CH₂Cl₂

Chemical Property of (C₁₂H₈N₂)Pd(C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)*CH₂Cl₂ = [(C₁₂H₈N₂)Pd(C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4*CH₂Cl₂

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Technology Process of (C₁₂H₈N₂)Pd(C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)*CH₂Cl₂ = [(C₁₂H₈N₂)Pd(C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4*CH₂Cl₂

There total 2 articles about (C₁₂H₈N₂)Pd(C(O)CH₃)(CO)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)*CH₂Cl₂ = [(C₁₂H₈N₂)Pd(C(O)CH₃)(CO)]B(C₆H₃(CF₃)2)4*CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

[Pd(CH3)(CO)(1,10-phenanthroline)][B(3,5-(CF3)2-C6H3)4] (160498-14-6) + carbon monoxide (201230-82-2) → (C12H8N2)Pd(C(O)CH3)(CO)(1+)*B(C6H3(CF3)2)4(1-)*CH2Cl2 = [(C12H8N2)Pd(C(O)CH3)(CO)]B(C6H3(CF3)2)4*CH2Cl2 (175857-99-5)

Guidance literature:

In dichloromethane; (Ar); CO purging (20°C, 1 min); crystn. on addn. of hexane to CH2Cl2 soln., slow cooling (-20°C, 1 h) and cooling (-78°C); elem. anal.; Kinetics;

DOI:10.1021/ja953276t

Reference yield: 6.5%

[(2)H6]acetone (666-52-4) + [Pd(CH3)(CO)(1,10-phenanthroline)][B(3,5-(CF3)2-C6H3)4] (160498-14-6) → (C12N2H8)Pd(CH3)(OC(C(2)H3)2)(1+)*B(C6H3(CF3)2)4(1-) = [(C12N2H8)Pd(CH3)(OC(C(2)H3)2)][B(C6H3(CF3)2)4] + (C12H8N2)Pd(C(O)CH3)(CO)(1+)*B(C6H3(CF3)2)4(1-)*CH2Cl2 = [(C12H8N2)Pd(C(O)CH3)(CO)]B(C6H3(CF3)2)4*CH2Cl2 (175857-99-5) + (C12H8N2)Pd(C(O)CH3)(OC(C((2)H)3)2)(1+)*B(C6H3(CF3)2)4(1-) = [(C12H8N2)Pd(COCH3)(OC(C((2)H)3)2)]B(C6H3(CF3)2)4 (175858-01-2)

Guidance literature:

(Ar); -78°C; Kinetics;

DOI:10.1021/ja953276t

upstream raw materials:

[⁽²⁾H₆]acetone

[Pd(CH₃)(CO)(1,10-phenanthroline)][B(3,5-(CF₃)2-C₆H₃)4]

carbon monoxide

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