n-butyl 3-nitrophenylether

Base Information

• Chemical Name: n-butyl 3-nitrophenylether
• CAS No.: 122329-01-5
• Molecular Formula: C₁₀H₁₃NO₃
• Molecular Weight: 195.218
• Mol file: 122329-01-5.mol

Synonyms:n-butyl 3-nitrophenylether

Chemical Property of n-butyl 3-nitrophenylether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of n-butyl 3-nitrophenylether

There total 5 articles about n-butyl 3-nitrophenylether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-bromo-butane (109-65-9) + meta-nitrophenol (554-84-7) → n-butyl 3-nitrophenylether (122329-01-5)

Guidance literature:

meta-nitrophenol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; for 0.0833333h; Inert atmosphere;

1-bromo-butane; In N,N-dimethyl-formamide; mineral oil; at 125 ℃; Inert atmosphere;

DOI:10.1016/j.bmc.2019.06.043

Reference yield: 96.0%

m-nitrobromobenzene (585-79-5) + butan-1-ol (71-36-3) → n-butyl 3-nitrophenylether (122329-01-5)

Guidance literature:

With palladium diacetate; caesium carbonate; 2-N,N-(dimethylamino)-2'-di-tert-butylphosphino-1,1'-binaphthyl; In toluene; at 70 ℃; for 14h;

DOI:10.1021/ja016863p

Reference yield: 94.0%

3-Nitrochlorobenzene (121-73-3) + butan-1-ol (71-36-3) → n-butyl 3-nitrophenylether (122329-01-5)

Guidance literature:

With palladium diacetate; caesium carbonate; 2-N,N-(dimethylamino)-2'-di-tert-butylphosphino-1,1'-binaphthyl; In toluene; at 70 ℃;

DOI:10.1021/ja016863p

upstream raw materials:

1-bromo-butane

meta-nitrophenol

1-iodo-butane

3-Nitrochlorobenzene

Downstream raw materials:

9-benzyl-6-(3-butoxyanilino)-2-chloro-9H-purine

2-(3-Butoxy-phenylamino)-6-oxo-1,6-dihydro-pyrimidine-5-carboxylic acid ethyl ester

2-(3-Butoxy-phenylamino)-6-oxo-1,6-dihydro-pyrimidine-5-carboxylic acid

3-butoxy-N,N-dimethyl-4-nitroso-aniline