5,5-diphenyl-2-<(4-nitrophenyl)imino>-3-isopropyl-4-thioxo-1,3-diazolidine

Base Information

Chemical Name:5,5-diphenyl-2-<(4-nitrophenyl)imino>-3-isopropyl-4-thioxo-1,3-diazolidine
CAS No.:128569-64-2
Molecular Formula:C₂₄H₂₂N₄O₂S
Molecular Weight:430.53
Hs Code.:

Synonyms:5,5-diphenyl-2-<(4-nitrophenyl)imino>-3-isopropyl-4-thioxo-1,3-diazolidine

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Chemical Property of 5,5-diphenyl-2-<(4-nitrophenyl)imino>-3-isopropyl-4-thioxo-1,3-diazolidine

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Technology Process of 5,5-diphenyl-2-<(4-nitrophenyl)imino>-3-isopropyl-4-thioxo-1,3-diazolidine

There total 4 articles about 5,5-diphenyl-2-<(4-nitrophenyl)imino>-3-isopropyl-4-thioxo-1,3-diazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 124512-17-0
4,5-dihydro-4,4-diphenyl-2-<(4-nitrophenhyl)amino>-5-(isopropylimino)thiazole

: 128569-64-2
5,5-diphenyl-2-<(4-nitrophenyl)imino>-3-isopropyl-4-thioxo-1,3-diazolidine

Guidance literature:: With 2,6-dichloro-benzonitrile; In acetonitrile; for 3h; Heating;
DOI:10.1021/jo00293a011

Reference yield:

: 1013-88-3
Benzophenone imine

: 128569-64-2
5,5-diphenyl-2-<(4-nitrophenyl)imino>-3-isopropyl-4-thioxo-1,3-diazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / tetrahydrofuran / 72 h / Ambient temperature

2: 84 percent / tetrahydrofuran / 22 h / Heating

3: 72 percent / DBN / acetonitrile / 3 h / Heating

With 2,6-dichloro-benzonitrile; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00293a011

Reference yield:

: 124512-04-5
1-Benzhydrylidene-3-(4-nitro-phenyl)-thiourea

: 128569-64-2
5,5-diphenyl-2-<(4-nitrophenyl)imino>-3-isopropyl-4-thioxo-1,3-diazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / tetrahydrofuran / 22 h / Heating

2: 72 percent / DBN / acetonitrile / 3 h / Heating

With 2,6-dichloro-benzonitrile; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00293a011