Technology Process of C26H18F6N2O5
There total 8 articles about C26H18F6N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: tetrahydrofuran / 20 °C
2.1: hydrazine hydrate / ethanol / 48 h / 20 °C
3.1: di-tert-butyl-diazodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C
3.2: 0.17 h / 20 °C
4.1: pyridine; copper diacetate / 1,2-dichloro-ethane / 48 h / 20 °C / Molecular sieve
5.1: hydrogen / 10 percent palladium on barium sulphate / methanol / 18 h / 25 °C / 760.05 Torr
6.1: pyridine; copper diacetate / dichloromethane / Molecular sieve
7.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
With
pyridine; di-tert-butyl-diazodicarboxylate; hydrogen; copper diacetate; hydrazine hydrate; triphenylphosphine; trifluoroacetic acid;
10 percent palladium on barium sulphate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; 1,2-dichloro-ethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine; copper diacetate / 1,2-dichloro-ethane / 48 h / 20 °C / Molecular sieve
2: hydrogen / 10 percent palladium on barium sulphate / methanol / 18 h / 25 °C / 760.05 Torr
3: pyridine; copper diacetate / dichloromethane / Molecular sieve
4: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
With
pyridine; hydrogen; copper diacetate; trifluoroacetic acid;
10 percent palladium on barium sulphate;
In
methanol; dichloromethane; 1,2-dichloro-ethane;