(1-hydroxy-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-yl)methanesulfonic acid

Base Information

Chemical Name:(1-hydroxy-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-yl)methanesulfonic acid
CAS No.:1196473-98-9
Molecular Formula:C₁₄H₁₃BO₆S
Molecular Weight:320.131
Hs Code.:

Synonyms:(1-hydroxy-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-yl)methanesulfonic acid

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Chemical Property of (1-hydroxy-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-yl)methanesulfonic acid

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Technology Process of (1-hydroxy-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-yl)methanesulfonic acid

There total 5 articles about (1-hydroxy-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-yl)methanesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1196473-99-0
methyl (1-hydroxy-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-yl)methanesulfonate

: 1196473-98-9
(1-hydroxy-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-yl)methanesulfonic acid

Guidance literature:: With sodium iodide; In acetone; at 20 ℃;

Reference yield:

: 59142-68-6
2-bromo-4-fluorobenzaldehyde

: 1196473-98-9
(1-hydroxy-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-yl)methanesulfonic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 20 - 100 °C

2.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 1.5 h / 80 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C

3.2: -78 - 20 °C

4.1: sodium iodide / acetone / 20 °C

With n-butyllithium; potassium acetate; potassium carbonate; sodium iodide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; hexane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1196474-92-6
2-bromo-4-phenoxybenzaldehyde

: 1196473-98-9
(1-hydroxy-6-phenoxy-1,3-dihydrobenzo[c][1,2]oxaborol-3-yl)methanesulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 1.5 h / 80 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C

2.2: -78 - 20 °C

3.1: sodium iodide / acetone / 20 °C

With n-butyllithium; potassium acetate; sodium iodide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; hexane; acetone;