1,1,3,5-pentanetetracarboxylic acid tetramethyl ester

Base Information

Chemical Name:1,1,3,5-pentanetetracarboxylic acid tetramethyl ester
CAS No.:36627-09-5
Molecular Formula:C₁₃H₂₀O₈
Molecular Weight:304.297
Hs Code.:

Synonyms:1,1,3,5-pentanetetracarboxylic acid tetramethyl ester

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Chemical Property of 1,1,3,5-pentanetetracarboxylic acid tetramethyl ester

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Technology Process of 1,1,3,5-pentanetetracarboxylic acid tetramethyl ester

There total 2 articles about 1,1,3,5-pentanetetracarboxylic acid tetramethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 5621-44-3
dimethyl 2-methylenepentanedioate

: 108-59-8
malonic acid dimethyl ester

: 36627-09-5
1,1,3,5-pentanetetracarboxylic acid tetramethyl ester

Guidance literature:: With tributylphosphine; In acetonitrile; at 20 ℃; for 23h; Inert atmosphere;
DOI:10.1055/s-0039-1690208

Reference yield:

: 5621-44-3
dimethyl 2-methylenepentanedioate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 108-59-8
malonic acid dimethyl ester

: 36627-09-5
1,1,3,5-pentanetetracarboxylic acid tetramethyl ester

: 1,3,3,5,7-heptanpentacarboxylic acid pentamethyl ester

Guidance literature:: dimethyl 2-methylenepentanedioate; With tetrabutylammomium bromide; potassium carbonate; In toluene; at 130 ℃;

malonic acid dimethyl ester; In toluene; for 6h;

acrylic acid methyl ester; In toluene; for 4h;