9-(p-hydroxyphenyl)-o-carborane

Base Information

Chemical Name:9-(p-hydroxyphenyl)-o-carborane
CAS No.:123462-83-9
Molecular Formula:C₈H₁₆B₁₀O
Molecular Weight:236.324
Hs Code.:

Synonyms:9-(p-hydroxyphenyl)-o-carborane

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Chemical Property of 9-(p-hydroxyphenyl)-o-carborane

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Technology Process of 9-(p-hydroxyphenyl)-o-carborane

There total 2 articles about 9-(p-hydroxyphenyl)-o-carborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.5%

: 123482-14-4
9-(p-methoxyphenyl)-o-carborane

: 123462-83-9
9-(p-hydroxyphenyl)-o-carborane

Guidance literature:: With hydrogen bromide; In acetic acid; N2 atmosphere; heating (140-150°C, 4 h); removal of solvent (vac.), treatment with water, extn. (ether), washing (water), drying (over Na2SO4), removal of ether, chromy. (benzene), sublimation (120-170°C, 1 mm), recrystn.;

Reference yield: 70.0%

: 17830-03-4
9-iodo-o-carborane

: 106-41-2
4-bromo-phenol

: 123462-83-9
9-(p-hydroxyphenyl)-o-carborane

Guidance literature:: With n-butyllithium; magnesium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; hexane; byproducts: phenol; N2; addn. of p-bromophenol in ether to BuLi in hexane (stirring, 0.dgree.C), stirring (23°C, 1 h), boiling (1.5 h), cooling (0°C), addn. of MgI2, stirring (0°C, 0.5 h), boiling (1 h), addn. of carborane and (PPh3)4Pd, boiling (30 h); pptn. on water addn. (0°C), washing (aq. HCl, water), removal of ether, extn. to removal of phenol (water, 50°C), drying (heating, vac.), chromy. (benzene), sublimation (120-170°C, 1mm), recrystn.; elem. anal.;