methyl (R)-2-{(tert-butoxycarbonyl)[3-(4-methoxybenzyl)pent-4-enyl]amino}acrylate

Base Information

Chemical Name:methyl (R)-2-{(tert-butoxycarbonyl)[3-(4-methoxybenzyl)pent-4-enyl]amino}acrylate
CAS No.:1105680-52-1
Molecular Formula:C₂₂H₃₁NO₅
Molecular Weight:389.492
Hs Code.:

Synonyms:methyl (R)-2-{(tert-butoxycarbonyl)[3-(4-methoxybenzyl)pent-4-enyl]amino}acrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (R)-2-{(tert-butoxycarbonyl)[3-(4-methoxybenzyl)pent-4-enyl]amino}acrylate

Chemical Property:

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Technology Process of methyl (R)-2-{(tert-butoxycarbonyl)[3-(4-methoxybenzyl)pent-4-enyl]amino}acrylate

There total 1 articles about methyl (R)-2-{(tert-butoxycarbonyl)[3-(4-methoxybenzyl)pent-4-enyl]amino}acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1105680-48-5
(R)-1-[2-(2-iodoethyl)but-3-enyl]-4-methoxybenzene

: 55477-80-0
methyl 2-[(tert-butoxycarbonyl)amino]acrylate

: 1105680-52-1
methyl (R)-2-{(tert-butoxycarbonyl)[3-(4-methoxybenzyl)pent-4-enyl]amino}acrylate

Guidance literature:: methyl 2-[(tert-butoxycarbonyl)amino]acrylate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 0.75h; Inert atmosphere;

(R)-1-[2-(2-iodoethyl)but-3-enyl]-4-methoxybenzene; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.200700308

Reference yield:

: 1105680-52-1
methyl (R)-2-{(tert-butoxycarbonyl)[3-(4-methoxybenzyl)pent-4-enyl]amino}acrylate

: 1105680-56-5
1-tert-butyl 2-methyl (R)-4-(4-methoxybenzyl)-5,6-dihydropyridine-1,2(4H)-dicarboxylate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 80 ℃; for 4h; optical yield given as %ee; Inert atmosphere;
DOI:10.1002/adsc.200700308