2-[N-benzyl-N'-(2,2,2-trifluoro-ethylidene)-hydrazino]-2-phenyl-ethanol

Base Information

• Chemical Name: 2-[N-benzyl-N'-(2,2,2-trifluoro-ethylidene)-hydrazino]-2-phenyl-ethanol
• CAS No.: 862090-31-1
• Molecular Formula: C₁₇H₁₇F₃N₂O
• Molecular Weight: 322.33

Synonyms:2-[N-benzyl-N'-(2,2,2-trifluoro-ethylidene)-hydrazino]-2-phenyl-ethanol

Chemical Property of 2-[N-benzyl-N'-(2,2,2-trifluoro-ethylidene)-hydrazino]-2-phenyl-ethanol

Chemical Property:

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Technology Process of 2-[N-benzyl-N'-(2,2,2-trifluoro-ethylidene)-hydrazino]-2-phenyl-ethanol

There total 2 articles about 2-[N-benzyl-N'-(2,2,2-trifluoro-ethylidene)-hydrazino]-2-phenyl-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(2R)-2-(N-Benzylhydrazino)-2-phenylethanol (216569-14-1) + ethyl trifluoroacetaldehyde hemiacetal (433-27-2) → 2-[N-benzyl-N'-(2,2,2-trifluoro-ethylidene)-hydrazino]-2-phenyl-ethanol (862090-31-1)

Guidance literature:

In toluene; for 0.583333h; Heating;

DOI:10.1016/j.tetlet.2005.05.040

Reference yield:

(2R)-2-(N-Benzylhydrazino)-2-phenylethanol (216569-14-1) + ethyl trifluoroacetaldehyde hemiacetal (433-27-2) → (R)-4-Benzyl-5-phenyl-2-trifluoromethyl-[1,3,4]oxadiazinane + 2-[N-benzyl-N'-(2,2,2-trifluoro-ethylidene)-hydrazino]-2-phenyl-ethanol (862090-31-1)

Guidance literature:

8-aminopyrene-1,3,6-trisulfonic acid, trisodium salt; In toluene; for 2h; Heating;

DOI:10.1016/j.tetlet.2005.05.040

Reference yield: 75.0%

2-[N-benzyl-N'-(2,2,2-trifluoro-ethylidene)-hydrazino]-2-phenyl-ethanol (862090-31-1) + vinylmagnesium chloride (3536-96-7) → 2-[N-benzyl-N'-(1-trifluoromethyl-allyl)-hydrazino]-2-phenyl-ethanol

Guidance literature:

In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 4h;

DOI:10.1016/j.tetlet.2005.05.040

upstream raw materials:

(2R)-2-(N-Benzylhydrazino)-2-phenylethanol

ethyl trifluoroacetaldehyde hemiacetal

Downstream raw materials:

2-[N-benzyl-N'-(1-trifluoromethyl-pentyl)-hydrazino]-2-phenyl-ethanol

(R)-N-benzyl-2-phenylglycinol

(2R,1'R)-2-<(1',2'-diphenylethyl)amino>-2-phenylethanol

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