C₂₆H₃₈O₄Si

Base Information

Chemical Name:C₂₆H₃₈O₄Si
CAS No.:1421598-64-2
Molecular Formula:C₂₆H₃₈O₄Si
Molecular Weight:442.671
Hs Code.:

C<sub>26</sub>H<sub>38</sub>O<sub>4</sub>Si

Synonyms:C₂₆H₃₈O₄Si

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Chemical Property of C₂₆H₃₈O₄Si

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Technology Process of C₂₆H₃₈O₄Si

There total 8 articles about C₂₆H₃₈O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1421598-63-1
C₂₆H₃₈O₃Si

: 1421598-64-2
C₂₆H₃₈O₄Si

Guidance literature:: With oxygen; copper(l) chloride; palladium dichloride; In water; N,N-dimethyl-formamide; for 17h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.12.033

Reference yield:

: 120743-99-9
p-[(tert-butyldimethylsilyl)oxy]benzaldehyde

: 1421598-64-2
C₂₆H₃₈O₄Si

Guidance literature:: Multi-step reaction with 6 steps

1: benzene / Inert atmosphere; Reflux

2: hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol / Inert atmosphere

3: diisobutylaluminium hydride / dichloromethane / -78 °C / Inert atmosphere

4: (R)-1,1'-Bi-2-naphthol; titanium(IV) isopropylate; trifluoroacetic acid / dichloromethane / -78 - -20 °C / Inert atmosphere; Molecular sieve

5: (1S)-10-camphorsulfonic acid / dichloromethane / 14 h / 20 °C / Inert atmosphere

6: palladium dichloride; copper(l) chloride; oxygen / N,N-dimethyl-formamide; water / 17 h / Inert atmosphere

With titanium(IV) isopropylate; 10 wt% Pd(OH)2 on carbon; (1S)-10-camphorsulfonic acid; hydrogen; oxygen; (R)-1,1'-Bi-2-naphthol; diisobutylaluminium hydride; trifluoroacetic acid; copper(l) chloride; palladium dichloride; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene; 4: |Keck Asymmetric Allylation / 6: |Wacker Oxidation;
DOI:10.1016/j.tetlet.2012.12.033

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1421598-64-2
C₂₆H₃₈O₄Si

Guidance literature:: Multi-step reaction with 7 steps

1: 1H-imidazole / dichloromethane / 0 °C / Inert atmosphere

2: benzene / Inert atmosphere; Reflux

3: hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol / Inert atmosphere

4: diisobutylaluminium hydride / dichloromethane / -78 °C / Inert atmosphere

5: (R)-1,1'-Bi-2-naphthol; titanium(IV) isopropylate; trifluoroacetic acid / dichloromethane / -78 - -20 °C / Inert atmosphere; Molecular sieve

6: (1S)-10-camphorsulfonic acid / dichloromethane / 14 h / 20 °C / Inert atmosphere

7: palladium dichloride; copper(l) chloride; oxygen / N,N-dimethyl-formamide; water / 17 h / Inert atmosphere

With 1H-imidazole; titanium(IV) isopropylate; 10 wt% Pd(OH)2 on carbon; (1S)-10-camphorsulfonic acid; hydrogen; oxygen; (R)-1,1'-Bi-2-naphthol; diisobutylaluminium hydride; trifluoroacetic acid; copper(l) chloride; palladium dichloride; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene; 5: |Keck Asymmetric Allylation / 7: |Wacker Oxidation;
DOI:10.1016/j.tetlet.2012.12.033