C₁₈H₁₇BrN₂O₂

Base Information

Chemical Name:C₁₈H₁₇BrN₂O₂
CAS No.:1242156-99-5
Molecular Formula:C₁₈H₁₇BrN₂O₂
Molecular Weight:373.249
Hs Code.:

C<sub>18</sub>H<sub>17</sub>BrN<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₈H₁₇BrN₂O₂

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Chemical Property of C₁₈H₁₇BrN₂O₂

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Technology Process of C₁₈H₁₇BrN₂O₂

There total 15 articles about C₁₈H₁₇BrN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1178884-33-7
6-dimethylamino-3,4-dihydro-2H-isoquinolin-1-one

: 67713-23-9
2,6-dibromobenzaldehyde

: 1242156-99-5
C₁₈H₁₇BrN₂O₂

Guidance literature:: With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 100 ℃; for 5.5h; Inert atmosphere;
DOI:10.1021/op4001077

Reference yield:

: 6-(dimethylamino)isoquinolin-1(2H)-one

: 1242156-99-5
C₁₈H₁₇BrN₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / ethanol

2: palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; caesium carbonate / 1,4-dioxane / 5.5 h / 100 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; ethanol; 2: |Buchwald-Hartwig Coupling;
DOI:10.1021/op4001077

Reference yield:

: 3-(DIMETHYLAMINO)-BENZENEPROPANOIC ACID

: 1242156-99-5
C₁₈H₁₇BrN₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide; chloroformic acid ethyl ester; triethylamine / acetone

2: toluene / 110 °C

3: aluminum (III) chloride / dichloromethane / 25 °C

4: palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; caesium carbonate / 1,4-dioxane / 5.5 h / 100 °C / Inert atmosphere

With aluminum (III) chloride; sodium azide; palladium diacetate; chloroformic acid ethyl ester; caesium carbonate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; dichloromethane; acetone; toluene; 2: |Curtius Rearrangement / 3: |Friedel-Crafts Acylation / 4: |Buchwald-Hartwig Coupling;
DOI:10.1021/op4001077