C₄₇H₇₃IN₁₀O₁₀

Base Information

Chemical Name:C₄₇H₇₃IN₁₀O₁₀
CAS No.:1316857-48-3
Molecular Formula:C₄₇H₇₃IN₁₀O₁₀
Molecular Weight:1065.06
Hs Code.:

C<sub>47</sub>H<sub>73</sub>IN<sub>10</sub>O<sub>10</sub>

Synonyms:C₄₇H₇₃IN₁₀O₁₀

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₇₃IN₁₀O₁₀

Chemical Property:

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Technology Process of C₄₇H₇₃IN₁₀O₁₀

There total 8 articles about C₄₇H₇₃IN₁₀O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1187357-11-4
N-(tert-butoxycarbonyl)-O-propargyl-1,3-aminopropanol

: C₃₆H₅₄IN₉O₇

: 1316857-48-3
C₄₇H₇₃IN₁₀O₁₀

Guidance literature:: With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 70 ℃; for 15h;
DOI:10.1039/c1ob05606a

Reference yield:

: 1316857-59-6
C₁₄H₁₇IO₄

: 1316857-48-3
C₄₇H₇₃IN₁₀O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride; methanol / 4 h / 50 °C

2: sodium hydroxide / water; dimethyl sulfoxide / 18 h / 25 °C

3: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 25 °C

4: triethylamine / dichloromethane / 4 h / 25 °C

5: sodium azide / N,N-dimethyl-formamide / 72 h / 110 °C

6: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 70 °C

With hydrogenchloride; methanol; copper(l) iodide; sodium azide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 3: Huisgen-Sharpless 1,3-dipolar cycloaddition / 6: Huisgen-Sharpless 1,3-dipolar cycloaddition;
DOI:10.1039/c1ob05606a

Reference yield:

: 1316857-42-7
C₁₂H₁₇IO₄

: 1316857-48-3
C₄₇H₇₃IN₁₀O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / water; dimethyl sulfoxide / 18 h / 25 °C

2: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 25 °C

3: triethylamine / dichloromethane / 4 h / 25 °C

4: sodium azide / N,N-dimethyl-formamide / 72 h / 110 °C

5: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 70 °C

With copper(l) iodide; sodium azide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 2: Huisgen-Sharpless 1,3-dipolar cycloaddition / 5: Huisgen-Sharpless 1,3-dipolar cycloaddition;
DOI:10.1039/c1ob05606a