racemic (R)-(+)-1-phenylethylcarbamic acid 2,6-di-sec-butylphenyl ester

Base Information

Chemical Name:racemic (R)-(+)-1-phenylethylcarbamic acid 2,6-di-sec-butylphenyl ester
CAS No.:1083093-43-9
Molecular Formula:C₂₃H₃₁NO₂
Molecular Weight:353.505
Hs Code.:

Synonyms:racemic (R)-(+)-1-phenylethylcarbamic acid 2,6-di-sec-butylphenyl ester

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Chemical Property of racemic (R)-(+)-1-phenylethylcarbamic acid 2,6-di-sec-butylphenyl ester

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Technology Process of racemic (R)-(+)-1-phenylethylcarbamic acid 2,6-di-sec-butylphenyl ester

There total 1 articles about racemic (R)-(+)-1-phenylethylcarbamic acid 2,6-di-sec-butylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 5510-99-6
2,6-di-sec-butylphenol

: 33375-06-3
(1R)-1-phenylethyl isocyanate

: 1083093-43-9
racemic (R)-(+)-1-phenylethylcarbamic acid 2,6-di-sec-butylphenyl ester

Guidance literature:: With dmap; In pyridine; at 100 ℃; Product distribution / selectivity;

Reference yield:

: 1083093-43-9
racemic (R)-(+)-1-phenylethylcarbamic acid 2,6-di-sec-butylphenyl ester

: 1083093-47-3
(R,R)-2,6-di-sec-butylphenol

Guidance literature:: racemic (R)-(+)-1-phenylethylcarbamic acid 2,6-di-sec-butylphenyl ester; In hexane; ethyl acetate; Resolution of racemate;

With sodium hydroxide; In 1,4-dioxane; water; at 70 ℃; for 0.25h;

With hydrogenchloride; In 1,4-dioxane; water; pH=3 - 4;