(S)-methyl 2-amino-3-(4-(2,3-dihydroxypropoxy)phenyl)propanoate hydrochloride

Base Information

Chemical Name:(S)-methyl 2-amino-3-(4-(2,3-dihydroxypropoxy)phenyl)propanoate hydrochloride
CAS No.:1071475-00-7
Molecular Formula:C₁₃H₁₉NO₅*ClH
Molecular Weight:305.759
Hs Code.:

Synonyms:(S)-methyl 2-amino-3-(4-(2,3-dihydroxypropoxy)phenyl)propanoate hydrochloride

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Chemical Property of (S)-methyl 2-amino-3-(4-(2,3-dihydroxypropoxy)phenyl)propanoate hydrochloride

Chemical Property:

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Technology Process of (S)-methyl 2-amino-3-(4-(2,3-dihydroxypropoxy)phenyl)propanoate hydrochloride

There total 2 articles about (S)-methyl 2-amino-3-(4-(2,3-dihydroxypropoxy)phenyl)propanoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1071474-99-1
(S)-methyl-2-(tert-butoxycarbonylamino)-3-(4-((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)phenyl)propanoate

: 1071475-00-7
(S)-methyl 2-amino-3-(4-(2,3-dihydroxypropoxy)phenyl)propanoate hydrochloride

Guidance literature:: (S)-methyl-2-(tert-butoxycarbonylamino)-3-(4-((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)phenyl)propanoate; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

With water; In 1,4-dioxane; methanol; at 20 ℃; for 2h;

Reference yield:

: 4326-36-7
(S)-N-(tert-butoxycarbonyl)tyrosine methyl ester

: 1071475-00-7
(S)-methyl 2-amino-3-(4-(2,3-dihydroxypropoxy)phenyl)propanoate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra(n-butyl)ammonium hydrogensulfate; caesium carbonate / N,N-dimethyl-formamide / 15 h / 70 - 75 °C

2.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

2.2: 2 h / 20 °C

With hydrogenchloride; tetra(n-butyl)ammonium hydrogensulfate; caesium carbonate; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 1071475-00-7
(S)-methyl 2-amino-3-(4-(2,3-dihydroxypropoxy)phenyl)propanoate hydrochloride

: 40224-49-5
(R)-2-azido-3-methylbutanoic acid

: 1071475-01-8
(S)-methyl-2-((S)-2-azido-3-methylbutanamido)-3-(4-(2,3-dihydroxypropoxy)phenyl)propanoate

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 15h;