3-trifluoromethylphenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:3-trifluoromethylphenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-galactopyranoside
CAS No.:911684-07-6
Molecular Formula:C₂₁H₂₃F₃O₉S
Molecular Weight:508.469
Hs Code.:

Synonyms:3-trifluoromethylphenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-galactopyranoside

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Chemical Property of 3-trifluoromethylphenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-galactopyranoside

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Technology Process of 3-trifluoromethylphenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-galactopyranoside

There total 1 articles about 3-trifluoromethylphenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 937-00-8
3-trifluoromethyl-thiophenol

: 4163-60-4
β-D-galactose peracetate

: 911684-07-6
3-trifluoromethylphenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-galactopyranoside

Guidance literature:: With tin(IV) chloride; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/ja063247q

Reference yield:

: 911684-07-6
3-trifluoromethylphenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-galactopyranoside

: (2R,3R,4S,5R,6S)-2-Hydroxymethyl-6-(3-trifluoromethyl-phenylsulfanyl)-tetrahydro-pyran-3,4,5-triol

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 2h;
DOI:10.1021/ja063247q

Reference yield:

: 911684-07-6
3-trifluoromethylphenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-galactopyranoside

: 911684-22-5
3-trifluoromethylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / methanol / 2 h / 20 °C

2: sodium hydride / dimethylformamide / 20 °C

With sodium methylate; sodium hydride; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja063247q