3-trifluoromethylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:3-trifluoromethylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside
CAS No.:911684-22-5
Molecular Formula:C₄₁H₃₉F₃O₅S
Molecular Weight:700.819
Hs Code.:

Synonyms:3-trifluoromethylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-trifluoromethylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside

Chemical Property:

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Technology Process of 3-trifluoromethylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside

There total 4 articles about 3-trifluoromethylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2R,3R,4S,5R,6S)-2-Hydroxymethyl-6-(3-trifluoromethyl-phenylsulfanyl)-tetrahydro-pyran-3,4,5-triol

: 100-39-0
benzyl bromide

: 911684-22-5
3-trifluoromethylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ja063247q

Reference yield:

: 911684-07-6
3-trifluoromethylphenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-galactopyranoside

: 911684-22-5
3-trifluoromethylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / methanol / 2 h / 20 °C

2: sodium hydride / dimethylformamide / 20 °C

With sodium methylate; sodium hydride; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja063247q

Reference yield:

: 937-00-8
3-trifluoromethyl-thiophenol

: 911684-22-5
3-trifluoromethylphenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / SnCl₄ / CH₂Cl₂ / 4 h / 20 °C

2: NaOMe / methanol / 2 h / 20 °C

3: sodium hydride / dimethylformamide / 20 °C

With sodium methylate; tin(IV) chloride; sodium hydride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja063247q