2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-isopropyl-phenylimino)methyl)phenol

Base Information

Chemical Name:2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-isopropyl-phenylimino)methyl)phenol
CAS No.:1392281-14-9
Molecular Formula:C₅₀H₅₃NO
Molecular Weight:683.977
Hs Code.:

Synonyms:2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-isopropyl-phenylimino)methyl)phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-isopropyl-phenylimino)methyl)phenol

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Technology Process of 2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-isopropyl-phenylimino)methyl)phenol

There total 1 articles about 2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-isopropyl-phenylimino)methyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.8%

: 37942-07-7
3,5-di-tert-butyl-2-hydroxybenzaldehyde

: 1333435-34-9
2,6-bis(diphenylmethyl)-4-isopropylphenylamine

: 1392281-14-9
2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-isopropyl-phenylimino)methyl)phenol

Guidance literature:: With toluene-4-sulfonic acid; In ethanol; for 12h; Reflux;
DOI:10.1016/j.jorganchem.2012.05.048

Reference yield: 97.0%

: 917-64-6
methyl magnesium iodide

: 60-29-7,927820-24-4
diethyl ether

: 1392281-14-9
2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-isopropyl-phenylimino)methyl)phenol

: C₅₄H₆₂IMgNO₂

Guidance literature:: In diethyl ether; at -60 - 20 ℃; for 15h; Concentration; Temperature;

Reference yield: 62.2%

: 31011-57-1,112925-19-6,112925-18-5
tetrachlorobis(tetrahydrofuran)titanium(IV)

: 1392281-14-9
2,4-di-tert-butyl-6-((2,6-dibenzhydryl-4-isopropyl-phenylimino)methyl)phenol

: 1392281-07-0
trichlorotitanium 2-((2,6-dibenzhydryl-4-isopropylphenylimino)methyl)-4,6-di-tert-butyl-phenoxylate tetrahydrofurane monosolvate

Guidance literature:: With KH; In toluene; N2, glove-box or Schlenk technique; to stirred soln. of iminophenol KH added at -78 °C, mixt. stirred for 3 h, TiCl4(THF)2 added at -78 °C, mixt. warmed to room temp., stirred for 24 h; solvent removed (vac.), extd. (CH2Cl2), filtrate concd. (vac.), recrystd. at -20 °C; elem. anal.;
DOI:10.1016/j.jorganchem.2012.05.048